[(PMe₂Ph)2PtPd(phenanthroline)B₁₀H₁₀]

Base Information

• Chemical Name: [(PMe₂Ph)2PtPd(phenanthroline)B₁₀H₁₀]
• CAS No.: 1039006-19-3
• Molecular Formula: C₂₈H₄₀B₁₀N₂P₂PdPt
• Molecular Weight: 876.197

Synonyms:

Chemical Property of [(PMe₂Ph)2PtPd(phenanthroline)B₁₀H₁₀]

Chemical Property:

Purity/Quality:

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Technology Process of [(PMe₂Ph)2PtPd(phenanthroline)B₁₀H₁₀]

There total 1 articles about [(PMe₂Ph)2PtPd(phenanthroline)B₁₀H₁₀] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

[PtCl2(PMe2Ph)2] (15393-14-3,38928-82-4,30759-88-7) + [(phenanthroline)PdB10H12] + potassium triethylborohydride → [(PMe2Ph)2PtPd(phenanthroline)B10H10] (1039006-19-3)

Guidance literature:

In tetrahydrofuran; toluene; byproducts: KCl; 1.0 M soln. of KHBEt3 (560 μmol) in thf added to toluene suspn. of Pdcomplex (280 μmol) (-70°C, stirring); warmed to -50°C; Pt complex (280 μmol) added; warmed to room temp. with stirring over night; filtered; recrystd. from 1,2-Cl2C2H4 by overlaying with C6H14;

DOI:10.1039/b800984h

Reference yield:

dichloromethane (75-09-2) + [(PMe2Ph)2PtPd(phenanthroline)B10H10] (1039006-19-3) + sulfur dioxide (7446-09-5,12143-17-8,89125-89-3) → [(PMe2Ph)2Pt(SO2)Pd(phenanthroline)B10H10]*3CH2Cl2

Guidance literature:

In dichloromethane; SO2 passed through soln. of metal complex; soln. overlayed with C6H14 (room temp.);

DOI:10.1039/b800984h

upstream raw materials:

[PtCl₂(PMe₂Ph)2]

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