Stannane, tributyl(3-phenyl-2-propenyl)-, (Z)-

Base Information

Chemical Name:Stannane, tributyl(3-phenyl-2-propenyl)-, (Z)-
CAS No.:130826-41-4
Molecular Formula:C₂₁H₃₆Sn
Molecular Weight:407.227
Hs Code.:

Synonyms:

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Chemical Property of Stannane, tributyl(3-phenyl-2-propenyl)-, (Z)-

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of Stannane, tributyl(3-phenyl-2-propenyl)-, (Z)-

There total 3 articles about Stannane, tributyl(3-phenyl-2-propenyl)-, (Z)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 4226-01-1
tri-n-butyltin lithium

: 2327-99-3
1-phenylpropadiene

: copper(l) cyanide

: 124582-43-0,131428-21-2
(E)-tributyl(1-phenylprop-1-en-2-yl)stannane

: 130826-41-4
(Z)-1-phenyl-3-(tributylstannyl)propene

Guidance literature:: With ammonium chloride; In tetrahydrofuran; (under Ar); addn. of CuCN to a soln. of the stannyllithium in THF at -78°C, dropwise addn. of the allene to this soln., stirring for 30 min, warming to 0°C, addn. of NH4Cl; extg., drying, chromy., elem. anal.;

Reference yield:

: 74785-32-3
(E)-cinnamyl(tributyl)tin

: 130826-41-4
(Z)-1-phenyl-3-(tributylstannyl)propene

: 19752-27-3,104108-28-3
1-phenylprop-2-enyl(tributyl)stannane

Guidance literature:: With 2,2,6,6-tetramethyl-piperidine-N-oxyl; In benzene; Irradiation (UV/VIS); N2; Sn-compd. soln. irradiation with 300 W high-pressure Hg lamp throughsatd. aq. CuSO4 soln. for 1 h, solvent evapn. (reduced pressure); TLC(PLC) (hexane/DCM 9:1); total yield 68 %, E/Z ratio 30:70;
DOI:10.1039/a707609f

Reference yield:

: 74785-32-3
(E)-cinnamyl(tributyl)tin

: 130826-41-4
(Z)-1-phenyl-3-(tributylstannyl)propene

: [1-(pyren-1-yl)prop-2-enyl]triphenylstannane

Guidance literature:: With 1,1-dibromomethane; In benzene; Irradiation (UV/VIS); N2; Sn-compd. soln. irradiation with 300 W high-pressure Hg lamp throughsatd. aq. CuSO4 soln. for 40 min, solvent evapn. (reduced pressure), Et 2O addn., soln. washing (aq. KF), drying (Na2SO4), evapn.; crystn. on residue treating with CHCl3/hexane at -20°C overnight;total yield 76 %, E/Z ratio 38:62;
DOI:10.1039/a707609f