cyclohex-3-enylmethyl acetate

Base Information

• Chemical Name: cyclohex-3-enylmethyl acetate
• CAS No.: 117266-97-4
• Molecular Formula: C₉H₁₄O₂
• Molecular Weight: 154.209

Synonyms:

Chemical Property of cyclohex-3-enylmethyl acetate

Chemical Property:

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Technology Process of cyclohex-3-enylmethyl acetate

There total 9 articles about cyclohex-3-enylmethyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

cyclohex-3-enylmethanol (72581-32-9,1679-51-2) + acetic anhydride (108-24-7) → cyclohex-3-enylmethyl acetate (117266-97-4,20144-30-3)

Guidance literature:

With H₃[P(Mo₃O₁₀)4]*nH₂O; at 20 ℃; for 0.0333333h;

DOI:10.1055/s-2007-1000859

Reference yield: 95.0%

cyclohex-3-enylmethanol (72581-32-9,1679-51-2) + ethyl acetate (141-78-6) → cyclohex-3-enylmethyl acetate (117266-97-4,20144-30-3)

Guidance literature:

With C₁₆H₂₅N₃O₂S; for 32h; Molecular sieve; Reflux;

DOI:10.1021/acscatal.9b01959

Reference yield: 85.0%

acetic anhydride (108-24-7) + 2-(Cyclohex-3-enylmethoxy)-tetrahydro-pyran (217438-57-8) → cyclohex-3-enylmethyl acetate (117266-97-4,20144-30-3)

Guidance literature:

With indium(III) triflate; In dichloromethane; at 0 - 20 ℃; for 1.16667h;

DOI:10.1016/S0040-4039(02)01864-6

upstream raw materials:

cyclohex-3-enylmethanol

acetic anhydride

acetic acid

2,3-Diazatricyclo<4.3.0.0^4,9>non-2-ene

Downstream raw materials:

4-Methylen-1-cyclohexen

1-methylcarbonyloxymethyl-3-cyclohexene oxide

Acetic acid (1S,3S,6R)-1-(7-oxa-bicyclo[4.1.0]hept-3-yl)methyl ester

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