2-(dimethylamino)-N,N-dimethyl-3,5-dinitrobenzamide

Base Information

Chemical Name:2-(dimethylamino)-N,N-dimethyl-3,5-dinitrobenzamide
CAS No.:53639-28-4
Molecular Formula:C₁₁H₁₄N₄O₅
Molecular Weight:282.256
Hs Code.:
DSSTox Substance ID:DTXSID201223857
ChEMBL ID:CHEMBL1322732

Synonyms:2-(dimethylamino)-N,N-dimethyl-3,5-dinitrobenzamide;53639-28-4;MLS000578711;CHEMBL1322732;DTXSID201223857;HMS2498A24;SMR000186203;SR-01000212303;SR-01000212303-1

Suppliers and Price of 2-(dimethylamino)-N,N-dimethyl-3,5-dinitrobenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(dimethylamino)-N,N-dimethyl-3,5-dinitrobenzamide

Chemical Property:

XLogP3:1.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:2
Exact Mass:282.09641956
Heavy Atom Count:20
Complexity:401

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CN(C)C1=C(C=C(C=C1[N+](=O)[O-])[N+](=O)[O-])C(=O)N(C)C

Technology Process of 2-(dimethylamino)-N,N-dimethyl-3,5-dinitrobenzamide

There total 5 articles about 2-(dimethylamino)-N,N-dimethyl-3,5-dinitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 102941-62-8
3,5-dinitro-2-(2-hydroxyethoxy)benzoic acid, methyl ester

: 124-40-3
dimethyl amine

: 53639-28-4
2-(dimethylamino)-3,5-dinitro-N,N-dimethylbenzamide

Guidance literature:: In water; for 8h; Ambient temperature;
DOI:10.1021/jo00365a031

Reference yield:

: 102941-62-8
3,5-dinitro-2-(2-hydroxyethoxy)benzoic acid, methyl ester

: 53639-28-4
2-(dimethylamino)-3,5-dinitro-N,N-dimethylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / methanol / 4 h / Ambient temperature

2: 90 percent / H₂O / 12 h / Ambient temperature

In methanol; water;
DOI:10.1021/jo00365a031

Reference yield:

: 102976-80-7
Meisenheimer complex A

: 53639-28-4
2-(dimethylamino)-3,5-dinitro-N,N-dimethylbenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / potassium thiphenoxide / methanol / 0.5 h / Ambient temperature

2: 90 percent / 20percent HCl / 1 h / Ambient temperature

3: 82 percent / H₂O / 8 h / Ambient temperature

With hydrogenchloride; potassium thiophenolate; In methanol; water;
DOI:10.1021/jo00365a031