C₅₀H₄₈N₄O₆S

Base Information

Chemical Name:C₅₀H₄₈N₄O₆S
CAS No.:1331747-84-2
Molecular Formula:C₅₀H₄₈N₄O₆S
Molecular Weight:833.02
Hs Code.:

C<sub>50</sub>H<sub>48</sub>N<sub>4</sub>O<sub>6</sub>S

Synonyms:

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Chemical Property of C₅₀H₄₈N₄O₆S

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Technology Process of C₅₀H₄₈N₄O₆S

There total 12 articles about C₅₀H₄₈N₄O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1194-02-1,143234-87-1
4-fluorobenzonitrile

: 1331747-82-0
benzyl 2-(benzyloxy)-4-(2-(N,4-dimethylphenylsulfonamido)-N-(4-(piperidin-4-yl)benzyl)acetamido)benzoate

: 1331747-84-2
C₅₀H₄₈N₄O₆S

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dimethyl sulfoxide; at 120 ℃; for 16h; Inert atmosphere;
DOI:10.1002/cmdc.201100194

Reference yield:

: 771-99-3
4-phenylpiperidine

: 1331747-84-2
C₅₀H₄₈N₄O₆S

Guidance literature:: Multi-step reaction with 7 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

2.1: aluminum (III) chloride / dichloromethane / 1 h / 0 °C / Inert atmosphere

3.1: palladium 10% on activated carbon; hydrogen; N-ethyl-N,N-diisopropylamine / ethyl acetate / 2 h / 20 °C

4.1: acetic acid / methanol / 3 h / 45 °C / Molecular sieve; Inert atmosphere

4.2: 12 h / 20 °C / Inert atmosphere

5.1: dichlorotriphenylphosphorane / chloroform / 12 h / 60 °C / Inert atmosphere

6.1: lithium hydroxide monohydrate; water / tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere

7.1: N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide / 16 h / 120 °C / Inert atmosphere

With aluminum (III) chloride; lithium hydroxide monohydrate; palladium 10% on activated carbon; water; hydrogen; acetic acid; N-ethyl-N,N-diisopropylamine; dichlorotriphenylphosphorane; In tetrahydrofuran; methanol; dichloromethane; chloroform; dimethyl sulfoxide; ethyl acetate; 2.1: Friedel Crafts acylation / 3.1: Rosenmund reduction;
DOI:10.1002/cmdc.201100194

Reference yield:

: 1241832-99-4
benzyl 4-amino-2-(benzyloxy)benzoate

: 1331747-84-2
C₅₀H₄₈N₄O₆S

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic acid / methanol / 3 h / 45 °C / Molecular sieve; Inert atmosphere

1.2: 12 h / 20 °C / Inert atmosphere

2.1: dichlorotriphenylphosphorane / chloroform / 12 h / 60 °C / Inert atmosphere

3.1: lithium hydroxide monohydrate; water / tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere

4.1: N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide / 16 h / 120 °C / Inert atmosphere

With lithium hydroxide monohydrate; water; acetic acid; N-ethyl-N,N-diisopropylamine; dichlorotriphenylphosphorane; In tetrahydrofuran; methanol; chloroform; dimethyl sulfoxide;
DOI:10.1002/cmdc.201100194