phenyl(3-phenyl-1,2,3,4-thiatriazol-3-ium-5-yl)amide

Base Information

Chemical Name:phenyl(3-phenyl-1,2,3,4-thiatriazol-3-ium-5-yl)amide
CAS No.:60077-87-4
Molecular Formula:C₁₃H₁₀N₄S
Molecular Weight:254.315
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenyl(3-phenyl-1,2,3,4-thiatriazol-3-ium-5-yl)amide

Chemical Property:

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Technology Process of phenyl(3-phenyl-1,2,3,4-thiatriazol-3-ium-5-yl)amide

There total 5 articles about phenyl(3-phenyl-1,2,3,4-thiatriazol-3-ium-5-yl)amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 3-phenyl-1,2,3,4-thiatriazolium-5-ethoxylate tetrafluoroborate

: 62-53-3
aniline

: 60077-87-4
phenyl(3-phenyl-1,2,3,4-thiatriazol-3-ium-5-yl)amide

Guidance literature:: With triethylamine; In acetonitrile; for 0.666667h; Reflux;
DOI:10.1002/anie.201708790

Reference yield:

: 60078-11-7
3-phenyl-1, 2, 3,4-oxatriazolium-5-thiolate

: 60077-87-4
phenyl(3-phenyl-1,2,3,4-thiatriazol-3-ium-5-yl)amide

Guidance literature:: Multi-step reaction with 3 steps

1: ammonia / ethanol / 0.5 h / Reflux

2: dichloromethane / 20 °C

3: triethylamine / acetonitrile / 0.67 h / Reflux

With ammonia; triethylamine; In ethanol; dichloromethane; acetonitrile;
DOI:10.1002/anie.201708790

Reference yield:

: 60078-16-2
3-phenyl-1-thia-2,3,4-thiatriazolium-5-olate

: 60077-87-4
phenyl(3-phenyl-1,2,3,4-thiatriazol-3-ium-5-yl)amide

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 20 °C

2: triethylamine / acetonitrile / 0.67 h / Reflux

With triethylamine; In dichloromethane; acetonitrile;
DOI:10.1002/anie.201708790