1,2-Benzenedicarbonitrile, 4,5-bis(pentyloxy)-

Base Information

Chemical Name:1,2-Benzenedicarbonitrile, 4,5-bis(pentyloxy)-
CAS No.:130996-05-3
Molecular Formula:C18H24N2O2
Molecular Weight:300.401
Hs Code.:
DSSTox Substance ID:DTXSID30470196
Wikidata:Q82298197

Synonyms:1,2-Benzenedicarbonitrile, 4,5-bis(pentyloxy)-;130996-05-3;4,5-dipent-oxyphthalonitrile;DTXSID30470196

Suppliers and Price of 1,2-Benzenedicarbonitrile, 4,5-bis(pentyloxy)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 1,2-Benzenedicarbonitrile, 4,5-bis(pentyloxy)-

Chemical Property:

XLogP3:4.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:10
Exact Mass:300.183778013
Heavy Atom Count:22
Complexity:354

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCOC1=C(C=C(C(=C1)C#N)C#N)OCCCCC

Technology Process of 1,2-Benzenedicarbonitrile, 4,5-bis(pentyloxy)-

There total 4 articles about 1,2-Benzenedicarbonitrile, 4,5-bis(pentyloxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: copper(l) cyanide

: 130996-04-2
1,2-Dibromo-4,5-bis(pentyloxy)benzene

: 177349-85-8
C₇₂H₉₆CuN₈O₈

: 130996-05-3
1,2-Dicyano-4,5-bis(pentyloxy)benzene

Guidance literature:: In N,N-dimethyl-formamide; at 150 ℃; for 12h; Inert atmosphere;
DOI:10.1142/S1088424611003264

Reference yield:

: 544-92-3
copper(I) cyanide

: 130996-04-2
1,2-Dibromo-4,5-bis(pentyloxy)benzene

: 130996-05-3
1,2-Dicyano-4,5-bis(pentyloxy)benzene

Guidance literature:: copper(I) cyanide; 1,2-Dibromo-4,5-bis(pentyloxy)benzene; In N,N-dimethyl-formamide; at 145 ℃; for 8h; Microwave irradiation;

With ammonium hydroxide; for 24h;

Reference yield:

: 110-53-2
1-Bromopentane

: 130996-05-3
1,2-Dicyano-4,5-bis(pentyloxy)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / 1) NaOMe / dimethylformamide / 1) 1h, r.t., 2) 3h, 110 deg C

2: 35.5 percent / dimethylformamide / 5 h / 150 °C

With sodium methylate; In N,N-dimethyl-formamide;