ethyl 2',4'-dichlorophenyl oxalate

Base Information

• Chemical Name: ethyl 2',4'-dichlorophenyl oxalate
• CAS No.: 93116-75-7
• Molecular Formula: C₁₀H₈Cl₂O₄
• Molecular Weight: 263.077
• Mol file: 93116-75-7.mol

Synonyms:

Chemical Property of ethyl 2',4'-dichlorophenyl oxalate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ethyl 2',4'-dichlorophenyl oxalate

There total 3 articles about ethyl 2',4'-dichlorophenyl oxalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

oxalic acid diethyl ester (95-92-1) + 2,4-dichlorophenol (120-83-2,40477-79-0) → ethyl 2',4'-dichlorophenyl oxalate (93116-75-7)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; for 4h; Heating;

DOI:10.1021/jf051458t

Reference yield:

Ethyl oxalyl chloride (4755-77-5) + 2,4-dichlorophenol (120-83-2,40477-79-0) → ethyl 2',4'-dichlorophenyl oxalate (93116-75-7)

Guidance literature:

With tetrachloromethane; sodium hydroxide;

DOI:10.1039/jr9540001388

Reference yield:

Ethyl dichloro-(ethoxy)-acetate (6957-89-7) + 2,4-dichlorophenol (120-83-2,40477-79-0) → ethyl 2',4'-dichlorophenyl oxalate (93116-75-7)

Guidance literature:

Heating;

upstream raw materials:

Ethyl oxalyl chloride

2,4-dichlorophenol

Ethyl dichloro-(ethoxy)-acetate

oxalic acid diethyl ester

Refernces