C₃₀H₄₄O₃

Base Information

• Chemical Name: C₃₀H₄₄O₃
• CAS No.: 1353054-45-1
• Molecular Formula: C₃₀H₄₄O₃
• Molecular Weight: 452.678
• Mol file: 1353054-45-1.mol

Synonyms:

Chemical Property of C₃₀H₄₄O₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₀H₄₄O₃

There total 5 articles about C₃₀H₄₄O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

4-(n-decyl)benzaldehyde (70972-99-5) + 4-(2-(tetrahydropyran-2-yloxy)ethyl)bromobenzene (79849-46-0) → C30H44O3 (1353054-45-1)

Guidance literature:

With n-butyllithium; at -78 ℃;

DOI:10.1016/j.bmc.2011.10.043

Reference yield:

4-decylbenzoyl chloride (54256-43-8) → C30H44O3 (1353054-45-1)

Guidance literature:

Multi-step reaction with 4 steps

1.1: dmap / 1 h / 20 °C

2.1: lithium aluminium tetrahydride / diethyl ether / 20 °C / Reflux

3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / -78 °C

3.2: 1.5 h / -78 - 20 °C

4.1: n-butyllithium / -78 °C

With dmap; lithium aluminium tetrahydride; n-butyllithium; oxalyl dichloride; dimethyl sulfoxide; In diethyl ether; dichloromethane; 3.1: Swern oxidation / 3.2: Swern oxidation;

DOI:10.1016/j.bmc.2011.10.043

Reference yield:

4-decylphenylmethanol (7408-29-9) → C30H44O3 (1353054-45-1)

Guidance literature:

Multi-step reaction with 2 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / -78 °C

1.2: 1.5 h / -78 - 20 °C

2.1: n-butyllithium / -78 °C

With n-butyllithium; oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; 1.1: Swern oxidation / 1.2: Swern oxidation;

DOI:10.1016/j.bmc.2011.10.043

upstream raw materials:

3,4-dihydro-2H-pyran

4-bromophenethanol

4-(n-decyl)benzaldehyde

4-(2-(tetrahydropyran-2-yloxy)ethyl)bromobenzene

Refernces