PD⁽³⁸⁾C₁₁₂₄

Base Information

Chemical Name:PD⁽³⁸⁾C₁₁₂₄
CAS No.:634586-78-0
Molecular Formula:C₃₅H₃₉N₅O₆
Molecular Weight:625.725
Hs Code.:

Synonyms:

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Chemical Property of PD⁽³⁸⁾C₁₁₂₄

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Technology Process of PD⁽³⁸⁾C₁₁₂₄

There total 9 articles about PD⁽³⁸⁾C₁₁₂₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 2.0%

: 1329063-32-2
C₄₂H₄₅N₅O₆

: 634586-78-0
PD⁽³⁸⁾C₁₁₂₄

Guidance literature:: With palladium 10% on activated carbon; hydrogen; acetic acid; In ethanol; under 760.051 Torr; Inert atmosphere;
DOI:10.1021/jm200608k

Reference yield:

: 329348-45-0
benzyl (S)-3-{[(tert-butoxy)carbonyl]amino}-4-phenylbutanoate

: 634586-78-0
PD⁽³⁸⁾C₁₁₂₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: trifluoroacetic acid / dichloromethane / 20 °C / Inert atmosphere

1.2: 1 h / Inert atmosphere

2.1: benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / dichloromethane / 0.25 h / 20 °C / Inert atmosphere

2.2: 3 h / Inert atmosphere

3.1: trifluoroacetic acid / dichloromethane / 20 °C / Inert atmosphere

3.2: 1 h / Inert atmosphere

4.1: benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / dichloromethane / 0.25 h / 20 °C / Inert atmosphere

4.2: 6 h / 20 °C / Inert atmosphere

5.1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C / Inert atmosphere

5.2: Inert atmosphere

6.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 6 h / 20 °C / Inert atmosphere

7.1: palladium 10% on activated carbon; hydrogen; acetic acid / ethanol / 760.05 Torr / Inert atmosphere

With palladium 10% on activated carbon; hydrogen; benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; acetic acid; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In ethanol; dichloromethane;
DOI:10.1021/jm200608k

Reference yield:

: 51871-62-6
(S)-3-tert-butoxycarbonylamino-4-phenylbutanoic acid

: 634586-78-0
PD⁽³⁸⁾C₁₁₂₄

Guidance literature:: Multi-step reaction with 8 steps

1.1: caesium carbonate / water; acetonitrile / 1 h / Inert atmosphere

1.2: Inert atmosphere

2.1: trifluoroacetic acid / dichloromethane / 20 °C / Inert atmosphere

2.2: 1 h / Inert atmosphere

3.1: benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / dichloromethane / 0.25 h / 20 °C / Inert atmosphere

3.2: 3 h / Inert atmosphere

4.1: trifluoroacetic acid / dichloromethane / 20 °C / Inert atmosphere

4.2: 1 h / Inert atmosphere

5.1: benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / dichloromethane / 0.25 h / 20 °C / Inert atmosphere

5.2: 6 h / 20 °C / Inert atmosphere

6.1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C / Inert atmosphere

6.2: Inert atmosphere

7.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 6 h / 20 °C / Inert atmosphere

8.1: palladium 10% on activated carbon; hydrogen; acetic acid / ethanol / 760.05 Torr / Inert atmosphere

With palladium 10% on activated carbon; hydrogen; benzotriazol-1-ol; caesium carbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; acetic acid; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In ethanol; dichloromethane; water; acetonitrile;
DOI:10.1021/jm200608k