(triphenylphosphine)AuSC₅H₄N

Base Information

Chemical Name:(triphenylphosphine)AuSC₅H₄N
CAS No.:385815-89-4
Molecular Formula:C₂₃H₁₉AuNPS
Molecular Weight:569.417
Hs Code.:

(triphenylphosphine)AuSC<sub>5</sub>H<sub>4</sub>N

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (triphenylphosphine)AuSC₅H₄N

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Technology Process of (triphenylphosphine)AuSC₅H₄N

There total 1 articles about (triphenylphosphine)AuSC₅H₄N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 4556-23-4
pyridine-4-thiol

: 14243-64-2
(triphenylphosphine)gold(I) chloride

: 385815-89-4
(triphenylphosphine)AuSC₅H₄N

Guidance literature:: With KOH; In dichloromethane; acetone; under N2 or Ar using Schlenk techniques; soln. of Au complex in CH2Cl2/acetone added to soln. of C5H4NSH in MeOH and KOH; mixt stirred overnightat room temp.; solvent removed; extd. (CH2Cl2); recrystd. (CH2Cl2/hexane); elem. anal.;
DOI:10.1016/S0020-1693(01)00543-6

Reference yield: 81.0%

: 385815-89-4
(triphenylphosphine)AuSC₅H₄N

: 14781-45-4
copper(II) hexafluoroacetylacetonate

: 71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1
benzene

: cis-[Cu(hexafluoroacetylacetonate)2((S-4-pyridine)AuPPh₃)2]*C₆H₆

Guidance literature:: In methanol; benzene; (Ar); standard Schlenk technique; soln. of Cu complex in methanol was added for 15 min with stirring to soln. of Au complex in C6H6; mixt. was stirred overnight at room temp.; solvent evapd. (vac.); recrystd. (C6H6/hexane); elem. anal.;
DOI:10.1016/j.jorganchem.2004.08.027

Reference yield: 25.0%

: 385815-89-4
(triphenylphosphine)AuSC₅H₄N

: Au₁₁(S-4-NC₅H₄)3(PPh₃)7

Guidance literature:: With NaBH₄; In ethanol; equimolar amts. of Au- and B-contg. compds. were mixed in EtOH with stirring at room temp. for 4 h; the mixt. was left standing at room temp. for 3 d; the ppt. was collected by filtration and dissolved in CH2Cl2; ethanol was added and then hexane to give single crystals; elem. anal.;
DOI:10.1016/j.jorganchem.2005.09.043