(C₆H₁₁)2BOCOCH₂NHCH₃

Base Information

• Chemical Name: (C₆H₁₁)2BOCOCH₂NHCH₃
• CAS No.: 117195-40-1
• Molecular Formula: C₁₅H₂₈BNO₂
• Molecular Weight: 265.204
• Mol file: 117195-40-1.mol

Synonyms:

Chemical Property of (C₆H₁₁)2BOCOCH₂NHCH₃

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of (C₆H₁₁)2BOCOCH₂NHCH₃

There total 1 articles about (C₆H₁₁)2BOCOCH₂NHCH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

sarcosine (107-97-1,25951-24-0) + B-methoxydicyclohexylborane (32705-46-7) → (C6H11)2BOCOCH2NHCH3 (117195-40-1)

Guidance literature:

In tetrahydrofuran; ethanol; water; dropwise addn. of 1 M soln. of (C6H11)2BOCH3 in THF to N-methylglycine in ethanol/H2O (1:1), stirring at 80-100°C; control of completion of the reaction by (11)B-NMR, removing of solvent under vacuum (1-2.0 mm), treating with methanol, obtaining viscous liquid;

DOI:10.1016/0022-328X(88)89064-8

upstream raw materials:

sarcosine

B-methoxydicyclohexylborane