Technology Process of C20H32N2O5S
There total 3 articles about C20H32N2O5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium tetrahydroborate;
In
dichloromethane;
for 12h;
Overall yield = 83 %; stereoselective reaction;
DOI:10.1002/ejoc.201300416
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium osmate(VI) dihydrate; benzyltriethylammonium bromide; (9S,9"S)-9,9"-[phthalazine-1,4-diylbis-(oxy)]bis[10,11-dihydro-6'-methoxycinchonane]; water / chloroform / 20 h / 33 °C / Schlenk technique; Inert atmosphere
2: sodium tetrahydroborate / dichloromethane / 12 h
With
potassium osmate(VI) dihydrate; sodium tetrahydroborate; water; benzyltriethylammonium bromide; (9S,9"S)-9,9"-[phthalazine-1,4-diylbis-(oxy)]bis[10,11-dihydro-6'-methoxycinchonane];
In
dichloromethane; chloroform;
DOI:10.1002/ejoc.201300416
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium osmate(VI) dihydrate; N-benzyl-N,N,N-triethylammonium chloride; water / chloroform / 20 h / 33 °C / Schlenk technique; Inert atmosphere
2: sodium tetrahydroborate / dichloromethane / 12 h
With
potassium osmate(VI) dihydrate; sodium tetrahydroborate; N-benzyl-N,N,N-triethylammonium chloride; water;
In
dichloromethane; chloroform;
DOI:10.1002/ejoc.201300416