Diazene, [4-[(6-bromohexyl)oxy]phenyl](4-nitrophenyl)-

Base Information

Chemical Name:Diazene, [4-[(6-bromohexyl)oxy]phenyl](4-nitrophenyl)-
CAS No.:131691-92-4
Molecular Formula:C18H20BrN3O3
Molecular Weight:406.279
Hs Code.:
DSSTox Substance ID:DTXSID90479862,DTXSID201043594
Nikkaji Number:J754.404I

Synonyms:Diazene, [4-[(6-bromohexyl)oxy]phenyl](4-nitrophenyl)-;131691-92-4;DTXSID90479862;DTXSID201043594;(E)-1-{4-[(6-Bromohexyl)oxy]phenyl}-2-(4-nitrophenyl)diazene;125769-27-9

Suppliers and Price of Diazene, [4-[(6-bromohexyl)oxy]phenyl](4-nitrophenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Diazene, [4-[(6-bromohexyl)oxy]phenyl](4-nitrophenyl)-

Chemical Property:

XLogP3:5.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:9
Exact Mass:405.06880
Heavy Atom Count:25
Complexity:401

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1N=NC2=CC=C(C=C2)OCCCCCCBr)[N+](=O)[O-]

Technology Process of Diazene, [4-[(6-bromohexyl)oxy]phenyl](4-nitrophenyl)-

There total 6 articles about Diazene, [4-[(6-bromohexyl)oxy]phenyl](4-nitrophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 629-03-8
1 ,6-dibromohexane

: 1435-60-5,81944-71-0
4-(4'-hydroxyphenylazo)nitrobenzene

: 131691-92-4
6-bromo 1-<4-(4-nitrophenylazo)phenoxy>hexane

Guidance literature:: With potassium carbonate; potassium iodide; In acetone; for 24h; Heating;
DOI:10.1016/j.tetlet.2005.02.005

Reference yield:

: 100-01-6,104810-17-5
4-nitro-aniline

: 131691-92-4
6-bromo 1-<4-(4-nitrophenylazo)phenoxy>hexane

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrochloric acid; sodium nitrite / cooling

1.2: 90 percent / aq. sodium hydroxide / 1 h / 5 °C

2.1: 60 percent / potassium carbonate / acetone / 100 h / Heating

With hydrogenchloride; potassium carbonate; sodium nitrite; In acetone;
DOI:10.1080/10587250008024848

Reference yield:

: 108-95-2,27073-41-2
phenol

: 131691-92-4
6-bromo 1-<4-(4-nitrophenylazo)phenoxy>hexane

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride; sodium nitrite / methanol; water / 1 h / 2 - 5 °C

1.2: 2 h / pH 8 - 9

2.1: potassium carbonate; potassium iodide / acetone / 24 h / Reflux; Inert atmosphere

With hydrogenchloride; potassium carbonate; potassium iodide; sodium nitrite; In methanol; water; acetone;
DOI:10.1016/j.molliq.2015.12.078