(+/-)-cis-4--3'-phenylspiro

Base Information

Chemical Name:(+/-)-cis-4--3'-phenylspiro
CAS No.:77330-09-7
Molecular Formula:C₂₃H₂₇NO₃
Molecular Weight:365.472
Hs Code.:

(+/-)-cis-4-<N-(ethoxycarbonyl)-N-methylamino>-3'-phenylspiro<cyclohexane-1,1'(3'H)-isobenzofuran>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-cis-4--3'-phenylspiro

Chemical Property:

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Technology Process of (+/-)-cis-4--3'-phenylspiro

There total 5 articles about (+/-)-cis-4--3'-phenylspiro which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 541-41-3
chloroformic acid ethyl ester

: 77329-94-3,77329-95-4,78262-65-4,78262-89-2
(+/-)-cis-4-(dimethylamino)-3'-phenylspiro

: 77330-09-7,77330-10-0,78263-24-8
(+/-)-cis-4--3'-phenylspiro

Guidance literature:: In dichloromethane;
DOI:10.1021/jm00137a025

Reference yield:

: 93-98-1,5705-51-1
N-phenyl benzoyl amide

: 77330-09-7,77330-10-0,78263-24-8
(+/-)-cis-4--3'-phenylspiro

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) n-BuLi / 1.) THF, hexane, 0 deg C, 1 h, 2.) THF, a) -40 deg C, 0.75 h, b) 0 deg C, 1 h

2: 32 percent / tetrahydrofuran; benzene; diethyl ether / 1 h / 0 °C

3: 61 percent / 97percent formic acid / 2 h / Heating

4: 27 percent / CH₂Cl₂

With n-butyllithium; formic acid; In tetrahydrofuran; diethyl ether; dichloromethane; benzene;
DOI:10.1021/jm00137a025

Reference yield:

: 40594-34-1
4-(dimethylamino)cyclohexanone

: 77330-09-7,77330-10-0,78263-24-8
(+/-)-cis-4--3'-phenylspiro

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) n-BuLi / 1.) THF, hexane, 0 deg C, 1 h, 2.) THF, a) -40 deg C, 0.75 h, b) 0 deg C, 1 h

2: 32 percent / tetrahydrofuran; benzene; diethyl ether / 1 h / 0 °C

3: 61 percent / 97percent formic acid / 2 h / Heating

4: 27 percent / CH₂Cl₂

With n-butyllithium; formic acid; In tetrahydrofuran; diethyl ether; dichloromethane; benzene;
DOI:10.1021/jm00137a025