(1'R,2R)-1--2-methylpyrrolidine

Base Information

Chemical Name:(1'R,2R)-1--2-methylpyrrolidine
CAS No.:135324-54-8
Molecular Formula:C₁₄H₂₂N₂O
Molecular Weight:234.341
Hs Code.:

(1'R,2R)-1-<N-(2-Hydroxy-1-phenylethyl)-N-methylamino>-2-methylpyrrolidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1'R,2R)-1--2-methylpyrrolidine

Chemical Property:

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Technology Process of (1'R,2R)-1--2-methylpyrrolidine

There total 6 articles about (1'R,2R)-1--2-methylpyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 135324-45-7
(1'R,2R)-1--2-methylpyrrolidine

: 74-88-4
methyl iodide

: 135324-54-8
(1'R,2R)-1--2-methylpyrrolidine

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; for 20h; Ambient temperature;
DOI:10.1248/cpb.39.836

Reference yield:

: 1603-79-8
phenylglyoxylic acid ethyl ester

: 135324-54-8
(1'R,2R)-1--2-methylpyrrolidine

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / 2 h / 60 °C

2: 28 percent / LiAlH₄ / tetrahydrofuran / 20 h / Ambient temperature

3: 68 percent / K₂CO₃ / dimethylformamide / 20 h / Ambient temperature

With lithium aluminium tetrahydride; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1248/cpb.39.836

Reference yield:

: 135324-43-5
(R)-1-Amino-2-methylpyrrolidine

: 135324-54-8
(1'R,2R)-1--2-methylpyrrolidine

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / 2 h / 60 °C

2: 28 percent / LiAlH₄ / tetrahydrofuran / 20 h / Ambient temperature

3: 68 percent / K₂CO₃ / dimethylformamide / 20 h / Ambient temperature

With lithium aluminium tetrahydride; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1248/cpb.39.836