Technology Process of C30H34Cl2N2S
There total 9 articles about C30H34Cl2N2S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium tris(acetoxy)borohydride; N-ethyl-N,N-diisopropylamine;
In
1,2-dichloro-ethane;
at 20 ℃;
DOI:10.1016/S0960-894X(00)00637-5
- Guidance literature:
-
Multi-step reaction with 8 steps
1: tetrahydrofuran / 20 °C
2: LAH / tetrahydrofuran / 20 °C
3: DIPEA / CH2Cl2 / 20 °C
4: OsO4; NMO / acetone; 2-methyl-propan-2-ol; H2O / 20 °C
5: aq. NaIO4 / tetrahydrofuran / 20 °C
6: NaBH(OAc)3; DIPEA / 1,2-dichloro-ethane / 20 °C
7: HCl / methanol / 20 °C
8: NaHB(OAc)3; DIPEA / 1,2-dichloro-ethane / 20 °C
With
hydrogenchloride; sodium periodate; osmium(VIII) oxide; lithium aluminium tetrahydride; N-methyl-2-indolinone; sodium tris(acetoxy)borohydride; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; methanol; dichloromethane; water; 1,2-dichloro-ethane; acetone; tert-butyl alcohol;
DOI:10.1016/S0960-894X(00)00637-5
- Guidance literature:
-
Multi-step reaction with 9 steps
1: (COCl)2; DMF / CH2Cl2 / 20 °C
2: tetrahydrofuran / 20 °C
3: LAH / tetrahydrofuran / 20 °C
4: DIPEA / CH2Cl2 / 20 °C
5: OsO4; NMO / acetone; 2-methyl-propan-2-ol; H2O / 20 °C
6: aq. NaIO4 / tetrahydrofuran / 20 °C
7: NaBH(OAc)3; DIPEA / 1,2-dichloro-ethane / 20 °C
8: HCl / methanol / 20 °C
9: NaHB(OAc)3; DIPEA / 1,2-dichloro-ethane / 20 °C
With
hydrogenchloride; sodium periodate; osmium(VIII) oxide; lithium aluminium tetrahydride; N-methyl-2-indolinone; oxalyl dichloride; sodium tris(acetoxy)borohydride; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide;
In
tetrahydrofuran; methanol; dichloromethane; water; 1,2-dichloro-ethane; acetone; tert-butyl alcohol;
DOI:10.1016/S0960-894X(00)00637-5