(1S,2S)-2-((R)-2-Hydroxy-propyl)-cyclohexanecarboxylic acid hydrazide

Base Information

Chemical Name:(1S,2S)-2-((R)-2-Hydroxy-propyl)-cyclohexanecarboxylic acid hydrazide
CAS No.:125258-98-2
Molecular Formula:C₁₀H₂₀N₂O₂
Molecular Weight:200.281
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,2S)-2-((R)-2-Hydroxy-propyl)-cyclohexanecarboxylic acid hydrazide

Chemical Property:

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Technology Process of (1S,2S)-2-((R)-2-Hydroxy-propyl)-cyclohexanecarboxylic acid hydrazide

There total 6 articles about (1S,2S)-2-((R)-2-Hydroxy-propyl)-cyclohexanecarboxylic acid hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 66122-70-1
3-methylisochroman-1-one

: 125258-98-2,125354-41-8,125354-42-9,125355-83-1
(1S,2S)-2-((R)-2-Hydroxy-propyl)-cyclohexanecarboxylic acid hydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 925 mg / H₂ / Pt₂O / acetic acid / 72 h / 760 Torr / Ambient temperature

2: 400 mg / hydrazine hydrate / ethanol / 0.25 h

With hydrogen; hydrazine hydrate; Adam’s catalyst; In ethanol; acetic acid;

Reference yield:

: 14736-49-3
2-(2-(methoxycarbonyl)phenyl)acetic acid

: 125258-98-2,125354-41-8,125354-42-9,125355-83-1
(1S,2S)-2-((R)-2-Hydroxy-propyl)-cyclohexanecarboxylic acid hydrazide

Guidance literature:: Multi-step reaction with 5 steps

1: 5.5 g / H₂ / Pt₂O / acetic acid; H₂O / 48 h / 2758.2 Torr / Ambient temperature

2: oxalyl chloride / benzene / Ambient temperature

3: 1.57 g / diethyl ether / Ambient temperature

4: 300 mg / NaBH₄ / methanol; H₂O / 1 h

5: 400 mg / hydrazine hydrate / ethanol / 0.25 h

With sodium tetrahydroborate; oxalyl dichloride; hydrogen; hydrazine hydrate; Adam’s catalyst; In methanol; diethyl ether; ethanol; water; acetic acid; benzene;