benzyl 3-(3-methoxycarbonylpropyl)-4-methylpyrrole-2-carboxylate

Base Information

Chemical Name:benzyl 3-(3-methoxycarbonylpropyl)-4-methylpyrrole-2-carboxylate
CAS No.:99602-65-0
Molecular Formula:C₁₈H₂₁NO₄
Molecular Weight:315.369
Hs Code.:

Synonyms:

Suppliers and Price of benzyl 3-(3-methoxycarbonylpropyl)-4-methylpyrrole-2-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of benzyl 3-(3-methoxycarbonylpropyl)-4-methylpyrrole-2-carboxylate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of benzyl 3-(3-methoxycarbonylpropyl)-4-methylpyrrole-2-carboxylate

There total 10 articles about benzyl 3-(3-methoxycarbonylpropyl)-4-methylpyrrole-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 67-56-1
methanol

: 99602-64-9
benzyl 3-(3-benzyloxycarbonylpropyl)-4-methylpyrrole-2-carboxylate

: 99602-65-0
benzyl 3-(3-methoxycarbonylpropyl)-4-methylpyrrole-2-carboxylate

Guidance literature:: With sodium methylate;

Reference yield:

: 2199-44-2
3,5-dimethyl-2-ethoxycarbonyl-1H-pyrrole

: 99602-65-0
benzyl 3-(3-methoxycarbonylpropyl)-4-methylpyrrole-2-carboxylate

Guidance literature:: Multi-step reaction with 10 steps

1: 95 percent / phenylmethanol / 0.5 h / 209 °C

2: 77 percent / SnCl₄ / CH₂Cl₂ / 0.25 h

3: 81 percent / sodium borohydride, BF₃*Et₂O / tetrahydrofuran / 0 deg C 15 min, methanol reflux 15 min

4: 79 percent / sulphuryl chloride / tetrahydrofuran / 0.5 h / Heating

5: 100 percent / diethyl ether

6: 96 percent / H₂ / palladized charcoal

7: 83 percent / iodine, potassium iodide

8: 94 percent / H₂ / Adams platinum

9: 68 percent / sodium benzyl oxide

10: 78 percent / sodium methoxide

With sodium tetrahydroborate; sulfuryl dichloride; boron trifluoride diethyl etherate; hydrogen; iodine; sodium methylate; tin(IV) chloride; sodium phenyl-methanolate; potassium iodide; platinum(IV) oxide; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; dichloromethane; benzyl alcohol;

Reference yield:

: 40236-19-9
benzyl 3,5-dimethylpyrrole-2-carboxylate

: 99602-65-0
benzyl 3-(3-methoxycarbonylpropyl)-4-methylpyrrole-2-carboxylate

Guidance literature:: Multi-step reaction with 9 steps

1: 77 percent / SnCl₄ / CH₂Cl₂ / 0.25 h

2: 81 percent / sodium borohydride, BF₃*Et₂O / tetrahydrofuran / 0 deg C 15 min, methanol reflux 15 min

3: 79 percent / sulphuryl chloride / tetrahydrofuran / 0.5 h / Heating

4: 100 percent / diethyl ether

5: 96 percent / H₂ / palladized charcoal

6: 83 percent / iodine, potassium iodide

7: 94 percent / H₂ / Adams platinum

8: 68 percent / sodium benzyl oxide

9: 78 percent / sodium methoxide

With sodium tetrahydroborate; sulfuryl dichloride; boron trifluoride diethyl etherate; hydrogen; iodine; sodium methylate; tin(IV) chloride; sodium phenyl-methanolate; potassium iodide; platinum(IV) oxide; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; dichloromethane;