1-benzyl-2-oxo-4-thioxo-1,2,3,4-tetrahydro-thiazolo[3,2-a][1,3,5]triazinylium betaine

Base Information

• Chemical Name: 1-benzyl-2-oxo-4-thioxo-1,2,3,4-tetrahydro-thiazolo[3,2-a][1,3,5]triazinylium betaine
• CAS No.: 39386-58-8
• Molecular Formula: C₁₂H₉N₃OS₂
• Molecular Weight: 275.355
• Mol file: 39386-58-8.mol

Synonyms:

Chemical Property of 1-benzyl-2-oxo-4-thioxo-1,2,3,4-tetrahydro-thiazolo[3,2-a][1,3,5]triazinylium betaine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-benzyl-2-oxo-4-thioxo-1,2,3,4-tetrahydro-thiazolo[3,2-a][1,3,5]triazinylium betaine

There total 1 articles about 1-benzyl-2-oxo-4-thioxo-1,2,3,4-tetrahydro-thiazolo[3,2-a][1,3,5]triazinylium betaine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-benzylthiazol-2-amine (41593-98-0) + Ethoxycarbonyl isothiocyanate (16182-04-0) → 1-benzyl-2-oxo-4-thioxo-1,2,3,4-tetrahydro-thiazolo[3,2-a][1,3,5]triazinylium betaine (39386-58-8)

Guidance literature:

In ethyl acetate;

DOI:10.1021/jo00962a011

Reference yield:

1-benzyl-2-oxo-4-thioxo-1,2,3,4-tetrahydro-thiazolo[3,2-a][1,3,5]triazinylium betaine (39386-58-8) → 2-benzylimino-thiazole-3-carbothioic acid amide (41594-05-2)

Guidance literature:

With water; In tetrahydrofuran;

DOI:10.1021/jo00962a011

Reference yield:

1-benzyl-2-oxo-4-thioxo-1,2,3,4-tetrahydro-thiazolo[3,2-a][1,3,5]triazinylium betaine (39386-58-8) → 2-benzylimino-thiazole-3-carbothioic acid ethylcarbamoyl-amide (41594-04-1)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂O / tetrahydrofuran

2: (i) NaH, THF, (ii) /BRN= 773743/

With water; In tetrahydrofuran;

DOI:10.1021/jo00962a011

upstream raw materials:

N-benzylthiazol-2-amine

Ethoxycarbonyl isothiocyanate

Downstream raw materials:

2-benzylimino-thiazole-3-carbothioic acid amide

2-benzylimino-thiazole-3-carbothioic acid ethylcarbamoyl-amide