tris(8-hydroxyquinoline) gallium

Base Information

Chemical Name:tris(8-hydroxyquinoline) gallium
CAS No.:136781-05-0
Molecular Formula:C₂₇H₁₈GaN₃O₃
Molecular Weight:502.181
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tris(8-hydroxyquinoline) gallium

Chemical Property:

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Technology Process of tris(8-hydroxyquinoline) gallium

There total 5 articles about tris(8-hydroxyquinoline) gallium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 148-24-3,24804-14-6
8-quinolinol

: 13450-90-3
Gallium trichloride

: 14642-34-3,136781-05-0,107984-00-9
tris(8-hydroxyquinoline) gallium

Guidance literature:: With ammonium hydroxide; In ethanol; byproducts: ammonium chloride; to the quinoline (85.17 mmol) in ethanol was added an ethanolic soln. of GaCl3 (28.39 mmol) dropwise; stirring at room temp. under N2 for 24 h;an excess of ammonium hydroxide was added dropwise; stirring for 1 h; the ppt. was vac. filtered and washed with water and ethanol; the product was dried under vac. and purified by vac. train sublimation;
DOI:10.1016/S0039-6028(00)00232-6

Reference yield:

: 148-24-3,24804-14-6
8-quinolinol

: gallium(III) nitrate hexahydrate

: 14642-34-3,136781-05-0,107984-00-9
tris(8-hydroxyquinoline) gallium

Guidance literature:: With ammonium acetate; In water; Ga salt was mixed with the aq. solution of the ligand buffered with ammonium acetate in a 1:3 molar ratio; recrystn. from MeOH; differential scanning calorimetry, thermal gravimetric anal.;
DOI:10.1021/ja010120m