Technology Process of C27H27BCl2N4O3
There total 5 articles about C27H27BCl2N4O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: hydrazine hydrate / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere
1.2: 18 h / 20 °C
2.1: potassium acetate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 18 h / 80 °C / Inert atmosphere
3.1: triethylamine; potassium phosphate tribasic trihydrate / bis-triphenylphosphine-palladium(II) chloride / 1,2-dimethoxyethane / 18 h / 80 °C / Inert atmosphere
4.1: potassium acetate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide
With
hydrazine hydrate; potassium phosphate tribasic trihydrate; potassium acetate; triethylamine;
bis-triphenylphosphine-palladium(II) chloride;
In
1,2-dimethoxyethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium acetate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 18 h / 80 °C / Inert atmosphere
2: triethylamine; potassium phosphate tribasic trihydrate / bis-triphenylphosphine-palladium(II) chloride / 1,2-dimethoxyethane / 18 h / 80 °C / Inert atmosphere
3: potassium acetate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide
With
potassium phosphate tribasic trihydrate; potassium acetate; triethylamine;
bis-triphenylphosphine-palladium(II) chloride;
In
1,2-dimethoxyethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylamine; potassium phosphate tribasic trihydrate / bis-triphenylphosphine-palladium(II) chloride / 1,2-dimethoxyethane / 18 h / 80 °C / Inert atmosphere
2: potassium acetate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide
With
potassium phosphate tribasic trihydrate; potassium acetate; triethylamine;
bis-triphenylphosphine-palladium(II) chloride;
In
1,2-dimethoxyethane; N,N-dimethyl-formamide;