C₄₀H₄₇NO₃Si

Base Information

Chemical Name:C₄₀H₄₇NO₃Si
CAS No.:1350911-02-2
Molecular Formula:C₄₀H₄₇NO₃Si
Molecular Weight:617.904
Hs Code.:

C<sub>40</sub>H<sub>47</sub>NO<sub>3</sub>Si

Synonyms:

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Chemical Property of C₄₀H₄₇NO₃Si

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Technology Process of C₄₀H₄₇NO₃Si

There total 9 articles about C₄₀H₄₇NO₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: C₃₁H₃₃NO₃Si

: 53273-28-2
dimethyl 2-oxo-3-cyclohexylpropylphosphonate

: 1350911-02-2
C₄₀H₄₇NO₃Si

Guidance literature:: With sodium hydride; at 20 ℃;
DOI:10.1016/j.bmcl.2011.09.004

Reference yield:

: 1350910-96-1
(1S,2R,3aS,8bS)-5,7-dibromo-1-(hydroxymethyl)-2,3,3a,8btetrahydro-1H-cyclopenta[b]benzofuran-2-ol

: 1350911-02-2
C₄₀H₄₇NO₃Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

2.1: isopropylmagnesium chloride / tetrahydrofuran

2.2: 60 °C

3.1: sodium hydride / 20 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / -10 °C

5.1: palladium on activated charcoal; hydrogen; sodium acetate / methanol / 20 °C

6.1: pyridine; dimethyl sulfoxide; dicyclohexyl-carbodiimide; trifluoroacetic acid / tetrahydrofuran / 20 °C

7.1: sodium hydride / 20 °C

With pyridine; 1H-imidazole; palladium on activated charcoal; tetrabutyl ammonium fluoride; hydrogen; isopropylmagnesium chloride; sodium acetate; sodium hydride; dimethyl sulfoxide; dicyclohexyl-carbodiimide; trifluoroacetic acid; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; 3.1: Horner-Wadsworth-Emmons olefination / 7.1: Horner-Wadsworth-Emmons olefination;
DOI:10.1016/j.bmcl.2011.09.004

Reference yield:

: 1350911-00-0
C₃₁H₃₅NO₃Si

: 1350911-02-2
C₄₀H₄₇NO₃Si

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; dimethyl sulfoxide; dicyclohexyl-carbodiimide; trifluoroacetic acid / tetrahydrofuran / 20 °C

2: sodium hydride / 20 °C

With pyridine; sodium hydride; dimethyl sulfoxide; dicyclohexyl-carbodiimide; trifluoroacetic acid; In tetrahydrofuran; 2: Horner-Wadsworth-Emmons olefination;
DOI:10.1016/j.bmcl.2011.09.004