Mn(GeCl₃)(CO)3[PC₆H₅(OC₂H₅)2]2

Base Information

Chemical Name:Mn(GeCl₃)(CO)3[PC₆H₅(OC₂H₅)2]2
CAS No.:1350766-91-4
Molecular Formula:C₂₃H₃₀Cl₃GeMnO₇P₂
Molecular Weight:714.322
Hs Code.:

Mn(GeCl<sub>3</sub>)(CO)3[PC<sub>6</sub>H<sub>5</sub>(OC<sub>2</sub>H<sub>5</sub>)2]2

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Chemical Property of Mn(GeCl₃)(CO)3[PC₆H₅(OC₂H₅)2]2

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Technology Process of Mn(GeCl₃)(CO)3[PC₆H₅(OC₂H₅)2]2

There total 2 articles about Mn(GeCl₃)(CO)3[PC₆H₅(OC₂H₅)2]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: germanium(II) chloride dioxane

: 941577-57-7
[MnCl(CO)3(P(C₆H₅)(OC₂H₅)2)2]

: 1350766-91-4
Mn(GeCl₃)(CO)3[PC₆H₅(OC₂H₅)2]2

Guidance literature:: In 1,2-dichloro-ethane; Schlenk techniques, inert atm.; excess of GeCl2*dioxane, reflux (90 min); solvent removed, oil triturated with EtOH, solid sepd. out from soln., crystn. (toluene, n-hexane); elem. anal.;
DOI:10.1016/j.jorganchem.2011.09.014

Reference yield: 80.0%

: 56-23-5
tetrachloromethane

: 1350766-95-8
Mn(GeH₃)(CO)3[PC₆H₅(OC₂H₅)2]2

: 1350766-91-4
Mn(GeCl₃)(CO)3[PC₆H₅(OC₂H₅)2]2

Guidance literature:: In toluene; Schlenk techniques, inert atm.; stirring at for 12 h; solvent removed, oil triturated with EtOH, solid sepd. out;
DOI:10.1016/j.jorganchem.2011.09.014

Reference yield: 65.0%

: 1350766-91-4
Mn(GeCl₃)(CO)3[PC₆H₅(OC₂H₅)2]2

: 75-16-1
methylmagnesium bromide

: 1350767-02-0
Mn(Ge(CH₃)3)(CO)3[PC₆H₅(OC₂H₅)2]2

Guidance literature:: In tetrahydrofuran; toluene; Schlenk techniques, inert atm.; excess of MgBrMe in THF added to mixt. of metal complex in toluene cooled to -196°C, reaching of room temp., stirring at room temp. for 3 h; solvent removed, extd. (toluene), evapn., oil triturated with n-hexane, solid sepd. out from soln., crystn. (toluene and hexane); elem. anal.;
DOI:10.1016/j.jorganchem.2011.09.014