lithium [(dimethylamino)methyl]trihydroborate

Base Information

• Chemical Name: lithium [(dimethylamino)methyl]trihydroborate
• CAS No.: 84280-42-2
• Molecular Formula: C₃H₁₁BN*Li
• Molecular Weight: 78.879
• Mol file: 84280-42-2.mol

Synonyms:

Chemical Property of lithium [(dimethylamino)methyl]trihydroborate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of lithium [(dimethylamino)methyl]trihydroborate

There total 2 articles about lithium [(dimethylamino)methyl]trihydroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

n-butyllithium (109-72-8) + trimethylamine borane (1231953-83-5) → lithium borohydride + lithium [butyl(trihydrido)borate] (82111-98-6) + lithium [(dimethylamino)methyl]trihydroborate (84280-42-2) + lithium benzyltrihydroborate (84280-43-3)

Guidance literature:

In hexane; toluene; under dry N2, refluxing for 30 min;

Reference yield:

n-butyllithium (109-72-8) + trimethylamine borane (1231953-83-5) → lithium borohydride + lithium [butyl(trihydrido)borate] (82111-98-6) + lithium [(dimethylamino)methyl]trihydroborate (84280-42-2) + lithium benzyltrihydroborate (84280-43-3) + (CH3)3N*H2B-n-C4H9

Guidance literature:

In hexane; toluene; under dry N2, treating H3B-NMe3 with n-BuLi (molar ratio 2:1) in hexane/toluene; not isolated, detected by NMR;

upstream raw materials:

n-butyllithium

trimethylamine borane