(S)-2-[(S)-2-(2-{2-[(S)-2-{(S)-2-Amino-6-[3-(2-chloro-ethyl)-ureido]-hexanoylamino}-3-(4-hydroxy-phenyl)-propionylamino]-acetylamino}-acetylamino)-3-phenyl-propionylamino]-4-methyl-pentanoic acid methyl ester; hydrochloride

Base Information

Chemical Name:(S)-2-[(S)-2-(2-{2-[(S)-2-{(S)-2-Amino-6-[3-(2-chloro-ethyl)-ureido]-hexanoylamino}-3-(4-hydroxy-phenyl)-propionylamino]-acetylamino}-acetylamino)-3-phenyl-propionylamino]-4-methyl-pentanoic acid methyl ester; hydrochloride
CAS No.:103310-89-0
Molecular Formula:C₃₈H₅₅ClN₈O₉*ClH
Molecular Weight:839.817
Hs Code.:

(S)-2-[(S)-2-(2-{2-[(S)-2-{(S)-2-Amino-6-[3-(2-chloro-ethyl)-ureido]-hexanoylamino}-3-(4-hydroxy-phenyl)-propionylamino]-acetylamino}-acetylamino)-3-phenyl-propionylamino]-4-methyl-pentanoic acid methyl ester; hydrochloride

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Chemical Property of (S)-2-[(S)-2-(2-{2-[(S)-2-{(S)-2-Amino-6-[3-(2-chloro-ethyl)-ureido]-hexanoylamino}-3-(4-hydroxy-phenyl)-propionylamino]-acetylamino}-acetylamino)-3-phenyl-propionylamino]-4-methyl-pentanoic acid methyl ester; hydrochloride

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Technology Process of (S)-2-[(S)-2-(2-{2-[(S)-2-{(S)-2-Amino-6-[3-(2-chloro-ethyl)-ureido]-hexanoylamino}-3-(4-hydroxy-phenyl)-propionylamino]-acetylamino}-acetylamino)-3-phenyl-propionylamino]-4-methyl-pentanoic acid methyl ester; hydrochloride

There total 4 articles about (S)-2-[(S)-2-(2-{2-[(S)-2-{(S)-2-Amino-6-[3-(2-chloro-ethyl)-ureido]-hexanoylamino}-3-(4-hydroxy-phenyl)-propionylamino]-acetylamino}-acetylamino)-3-phenyl-propionylamino]-4-methyl-pentanoic acid methyl ester; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2389-46-0
N-α-tert-butyloxycarbonyl-N-ε-benzyloxycarbonyl-lysine p-nitrophenyl ester

: 103310-89-0
(S)-2-[(S)-2-(2-{2-[(S)-2-{(S)-2-Amino-6-[3-(2-chloro-ethyl)-ureido]-hexanoylamino}-3-(4-hydroxy-phenyl)-propionylamino]-acetylamino}-acetylamino)-3-phenyl-propionylamino]-4-methyl-pentanoic acid methyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 88.5 percent / pyridine / 24 h / Ambient temperature

2: 77.8 percent / H₂ / Pd/C / methanol / 2 h

3: 50 percent / dimethylformamide / Ambient temperature

4: 80 percent / 2N HCl / ethyl acetate / 0.5 h / Ambient temperature

With hydrogenchloride; hydrogen; palladium on activated charcoal; In pyridine; methanol; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 63441-70-3
Leu-enkephalin methyl ester

: 103310-89-0
(S)-2-[(S)-2-(2-{2-[(S)-2-{(S)-2-Amino-6-[3-(2-chloro-ethyl)-ureido]-hexanoylamino}-3-(4-hydroxy-phenyl)-propionylamino]-acetylamino}-acetylamino)-3-phenyl-propionylamino]-4-methyl-pentanoic acid methyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 88.5 percent / pyridine / 24 h / Ambient temperature

2: 77.8 percent / H₂ / Pd/C / methanol / 2 h

3: 50 percent / dimethylformamide / Ambient temperature

4: 80 percent / 2N HCl / ethyl acetate / 0.5 h / Ambient temperature

With hydrogenchloride; hydrogen; palladium on activated charcoal; In pyridine; methanol; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 84047-89-2
(S)-2-[(S)-2-(2-{2-[(S)-2-((S)-6-Benzyloxycarbonylamino-2-tert-butoxycarbonylamino-hexanoylamino)-3-(4-hydroxy-phenyl)-propionylamino]-acetylamino}-acetylamino)-3-phenyl-propionylamino]-4-methyl-pentanoic acid methyl ester

: 103310-89-0
(S)-2-[(S)-2-(2-{2-[(S)-2-{(S)-2-Amino-6-[3-(2-chloro-ethyl)-ureido]-hexanoylamino}-3-(4-hydroxy-phenyl)-propionylamino]-acetylamino}-acetylamino)-3-phenyl-propionylamino]-4-methyl-pentanoic acid methyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 77.8 percent / H₂ / Pd/C / methanol / 2 h

2: 50 percent / dimethylformamide / Ambient temperature

3: 80 percent / 2N HCl / ethyl acetate / 0.5 h / Ambient temperature

With hydrogenchloride; hydrogen; palladium on activated charcoal; In methanol; ethyl acetate; N,N-dimethyl-formamide;