trans-(Fe(η2-H2)(H)((C2H5)2PCH2CH2P(C2H5)2)2)BPh4

Base Information

Chemical Name:trans-(Fe(η2-H2)(H)((C2H5)2PCH2CH2P(C2H5)2)2)BPh4
CAS No.:108150-67-0
Molecular Formula:C₂₀H₅₁FeP₄*C₂₄H₂₀B
Molecular Weight:790.601
Hs Code.:

Synonyms:

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Chemical Property of trans-(Fe(η2-H2)(H)((C2H5)2PCH2CH2P(C2H5)2)2)BPh4

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Technology Process of trans-(Fe(η2-H2)(H)((C2H5)2PCH2CH2P(C2H5)2)2)BPh4

There total 5 articles about trans-(Fe(η2-H2)(H)((C2H5)2PCH2CH2P(C2H5)2)2)BPh4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 16940-66-2
sodium tetrahydroborate

: 123931-96-4,22920-46-3,133322-11-9
dichlorobis(ethane-1,2-bis(diethylphosphine-P))iron(II)

: 143-66-8
sodium tetraphenyl borate

: 108150-67-0
trans-(Fe(η2-H2)(H)((C2H5)2PCH2CH2P(C2H5)2)2)BPh4

Guidance literature:: In ethanol; under Ar, Fe-compd. in EtOH treated with NaBH4 for 15 min, addn. of NaBPh4 in EtOH, stirred for 2 h; filtered off, dried in vac.;
DOI:10.1039/DT9930003151

Reference yield:

: 123931-96-4,22920-46-3,133322-11-9
dichlorobis(ethane-1,2-bis(diethylphosphine-P))iron(II)

: 143-66-8
sodium tetraphenyl borate

: 108150-67-0
trans-(Fe(η2-H2)(H)((C2H5)2PCH2CH2P(C2H5)2)2)BPh4

Guidance literature:: With H₂; NaOCH₂CH₃; In ethanol; addn. (via syringe) of NaOEt/EtOH to NaBPh4 in EtOH, cooling to 14°C, addn. of Fe-complex, placing under H2, color change from light green to yellow, then the soln. becomes clear, pptn. of white product; filtration, washing with EtOH, then H2O, then diethyl ether;