(C₆H₁₁)2BOCOCH₂NH₂

Base Information

Chemical Name:(C₆H₁₁)2BOCOCH₂NH₂
CAS No.:117256-71-0
Molecular Formula:C₁₄H₂₆BNO₂
Molecular Weight:251.177
Hs Code.:

(C<sub>6</sub>H<sub>11</sub>)2BOCOCH<sub>2</sub>NH<sub>2</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (C₆H₁₁)2BOCOCH₂NH₂

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Technology Process of (C₆H₁₁)2BOCOCH₂NH₂

There total 1 articles about (C₆H₁₁)2BOCOCH₂NH₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 32705-46-7
B-methoxydicyclohexylborane

: 56-40-6,18875-39-3,25718-94-9
glycine

: 117256-71-0
(C₆H₁₁)2BOCOCH₂NH₂

Guidance literature:: In tetrahydrofuran; dimethyl sulfoxide; dropwise addn. of 1 M soln. of (C6H11)2BOCH3 in THF to glycine in DMSO, stirring at 80-100°C; control of completion of the reaction by (11)B-NMR, removing of solvent under vacuum (1-2.0 mm), treating with methanol, filtration, washing with hexane or ether;
DOI:10.1016/0022-328X(88)89064-8