FeI₂(CO)((C₆H₅)2PCH₂P(C₆H₅)2)2

Base Information

Chemical Name:FeI₂(CO)((C₆H₅)2PCH₂P(C₆H₅)2)2
CAS No.:110981-64-1
Molecular Formula:C₅₁H₄₄FeI₂OP₄
Molecular Weight:1106.46
Hs Code.:

FeI<sub>2</sub>(CO)((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)2

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of FeI₂(CO)((C₆H₅)2PCH₂P(C₆H₅)2)2

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Technology Process of FeI₂(CO)((C₆H₅)2PCH₂P(C₆H₅)2)2

There total 1 articles about FeI₂(CO)((C₆H₅)2PCH₂P(C₆H₅)2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 7439-89-6
iron

: 2071-20-7
bis-diphenylphosphinomethane

: 110981-64-1
FeI₂(CO)((C₆H₅)2PCH₂P(C₆H₅)2)2

Guidance literature:: With carbon monoxide; I₂; In tetrahydrofuran; Fe and I2 were refluxed in THF for 2 h, cooling, CO was bubbled throughsoln., dppm was added, mixt. was stirred under CO for 0.5 h; Et2O was added, ppt. was isolated by filtration, washed with THF-Et2O, Et2O, dried in vacuo; elem. anal.;
DOI:10.1039/DT9870002005

Reference yield: 29.0%

: 110981-64-1
FeI₂(CO)((C₆H₅)2PCH₂P(C₆H₅)2)2

: 32005-36-0
bis(dibenzylideneacetone)-palladium⁽⁰⁾

: 67477-87-6
Pd2I2(μ-dpm)2

: 110981-66-3
IFe(CO)2((C₆H₅)2PCH₂P(C₆H₅)2)2PdI

Guidance literature:: With carbon monoxide; In benzene; Pd- and Fe-complexes were stirred together in benzene with CO bubbling through the soln. for 3 h; filtered, excess of Et2O was added to the filtrate, mixt. was refrigerated (5°C) overnight, in cases when crystals of heterobimetallic complex were contaminated with Pd2-compound (identified by (31)P NMR), mixt. was sepd. manually; elem. anal.;
DOI:10.1039/DT9870002005