(2,2',2''-tris(4-tert-butylphenylamino)triethylamine)WMe

Base Information

Chemical Name:(2,2',2''-tris(4-tert-butylphenylamino)triethylamine)WMe
CAS No.:351029-46-4
Molecular Formula:C₃₇H₅₄N₄W
Molecular Weight:738.713
Hs Code.:

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Chemical Property of (2,2',2''-tris(4-tert-butylphenylamino)triethylamine)WMe

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Technology Process of (2,2',2''-tris(4-tert-butylphenylamino)triethylamine)WMe

There total 1 articles about (2,2',2''-tris(4-tert-butylphenylamino)triethylamine)WMe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 146733-16-6
tetrachloro(1,2-dimethoxyethane-O,O')tungsten(IV)

: 219598-39-7
2,2',2''-tris(phenylamino)triethylamine

: 676-58-4
methylmagnesium chloride

: 351029-46-4
(2,2',2''-tris(4-tert-butylphenylamino)triethylamine)WMe

Guidance literature:: In tetrahydrofuran; byproducts: MgCl2(dioxane); under N2 atm. WCl4(DME) was added to soln. amine in THF, stirred for 30 min., cooled to -35°C, MeMgCl in THF was added, react. mixt. was allowed to warm to room temp. for 1 h; solvent was removed, residue was dissolved in toluene, 1,4-dioxane was added, filtered, evapd., residue was dissolved in Et2O, cooled to -35°C, crystals were collected, washed with pentane, and dried in vacuo;elem. anal.;
DOI:10.1021/ic001122v