1'-methyl-2,3-diphenylspiroindol>-2'(1'H)-one

Base Information

Chemical Name:1'-methyl-2,3-diphenylspiroindol>-2'(1'H)-one
CAS No.:81276-66-6
Molecular Formula:C₂₃H₁₉NO
Molecular Weight:325.41
Hs Code.:

1'-methyl-2,3-diphenylspiro<cyclopropane-1,3'-<3H>indol>-2'(1'H)-one

Synonyms:

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Chemical Property of 1'-methyl-2,3-diphenylspiroindol>-2'(1'H)-one

Chemical Property:

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Technology Process of 1'-methyl-2,3-diphenylspiroindol>-2'(1'H)-one

There total 5 articles about 1'-methyl-2,3-diphenylspiroindol>-2'(1'H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1-methylspiro<3H-indol-3,2'-oxiran>-2(1H)-one

: 41570-67-6
1-benzyltetrahydro-1H-thiophen-1-ium bromide

: C₂₃H₁₉NO

: 81276-66-6
1'-methyl-2,3-diphenylspiroindol>-2'(1'H)-one

Guidance literature:: With sodium hydride; In dimethyl sulfoxide; at 25 ℃; for 2h; Overall yield = 30 %; Overall yield = 0.054 g; Inert atmosphere;
DOI:10.1021/acs.orglett.8b01840

Reference yield:

: 1-(tert-butylsulfonyl)-1'-methylspiro[aziridine-2,3'-indolin]-2'-one

: 41570-67-6
1-benzyltetrahydro-1H-thiophen-1-ium bromide

: C₂₃H₁₉NO

: 81276-66-6
1'-methyl-2,3-diphenylspiroindol>-2'(1'H)-one

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 6h; Overall yield = 68 %; Overall yield = 0.026 g; Inert atmosphere;
DOI:10.1021/acs.orglett.8b01840

Reference yield:

: 41570-67-6
1-benzyltetrahydro-1H-thiophen-1-ium bromide

: 59181-30-5
3-benzylidene-1H-pyrrolo[2,3-b]pyridin-2(3H)-one

: C₂₃H₁₉NO

: 81276-66-6
1'-methyl-2,3-diphenylspiroindol>-2'(1'H)-one

Guidance literature:: With sodium hydride; In dimethyl sulfoxide; at 25 ℃; for 4h; Overall yield = 60 %; Overall yield = 0.108 g; Inert atmosphere;
DOI:10.1021/acs.orglett.8b01840