5-[1-(3,5-Dimethoxy-2-nitro-phenyl)-meth-(Z)-ylidene]-6-methyl-5,6,7,8-tetrahydro-[1,3]dioxolo[4,5-g]isoquinoline

Base Information

Chemical Name:5-[1-(3,5-Dimethoxy-2-nitro-phenyl)-meth-(Z)-ylidene]-6-methyl-5,6,7,8-tetrahydro-[1,3]dioxolo[4,5-g]isoquinoline
CAS No.:131653-14-0
Molecular Formula:C₂₀H₂₀N₂O₆
Molecular Weight:384.389
Hs Code.:

Synonyms:

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Chemical Property of 5-[1-(3,5-Dimethoxy-2-nitro-phenyl)-meth-(Z)-ylidene]-6-methyl-5,6,7,8-tetrahydro-[1,3]dioxolo[4,5-g]isoquinoline

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Technology Process of 5-[1-(3,5-Dimethoxy-2-nitro-phenyl)-meth-(Z)-ylidene]-6-methyl-5,6,7,8-tetrahydro-[1,3]dioxolo[4,5-g]isoquinoline

There total 9 articles about 5-[1-(3,5-Dimethoxy-2-nitro-phenyl)-meth-(Z)-ylidene]-6-methyl-5,6,7,8-tetrahydro-[1,3]dioxolo[4,5-g]isoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 131653-13-9
5-(3,5-Dimethoxy-2-nitro-benzyl)-6-methyl-7,8-dihydro-[1,3]dioxolo[4,5-g]isoquinolin-6-ium; iodide

: 131653-14-0
5-[1-(3,5-Dimethoxy-2-nitro-phenyl)-meth-(Z)-ylidene]-6-methyl-5,6,7,8-tetrahydro-[1,3]dioxolo[4,5-g]isoquinoline

Guidance literature:: With hydrogenchloride; poudre de zinc; water; acetic acid; for 1h;

Reference yield:

: 2150-37-0
methyl 3,5-dimethoxybenzoate

: 131653-14-0
5-[1-(3,5-Dimethoxy-2-nitro-phenyl)-meth-(Z)-ylidene]-6-methyl-5,6,7,8-tetrahydro-[1,3]dioxolo[4,5-g]isoquinoline

Guidance literature:: Multi-step reaction with 8 steps

1: acide nitrique fumant, anhydride acetique / -20 °C

2: 98.5 percent / aq. KOH / methanol / 0.5 h / Heating

3: SOCl₂, triethylamine / benzene / 3 h / Heating

4: triethylamine / diethyl ether

5: benzoate d'argent, triethylamine / diethyl ether; acetonitrile

6: Roblot F_., Hocquemiller R_., Cave A_., J_. Chem_. Research ⁽¹⁹⁸⁹⁾ (S) 344-345 (M) 2637-2651

7: 75 percent / CHCl₃ / Heating

8: 100 percent / acide acetique, H₂O, 12 N HCl, poudre de zinc / 1 h

With hydrogenchloride; potassium hydroxide; thionyl chloride; acide nitrique fumant; benzoate d'argent; poudre de zinc; water; acetic anhydride; acetic acid; triethylamine; In methanol; diethyl ether; chloroform; acetonitrile; benzene;

Reference yield:

: 109069-76-3
3,5-dimethoxy-2-nitrobenzoyl chloride

: 131653-14-0
5-[1-(3,5-Dimethoxy-2-nitro-phenyl)-meth-(Z)-ylidene]-6-methyl-5,6,7,8-tetrahydro-[1,3]dioxolo[4,5-g]isoquinoline

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine / diethyl ether

2: benzoate d'argent, triethylamine / diethyl ether; acetonitrile

3: Roblot F_., Hocquemiller R_., Cave A_., J_. Chem_. Research ⁽¹⁹⁸⁹⁾ (S) 344-345 (M) 2637-2651

4: 75 percent / CHCl₃ / Heating

5: 100 percent / acide acetique, H₂O, 12 N HCl, poudre de zinc / 1 h

With hydrogenchloride; benzoate d'argent; poudre de zinc; water; acetic acid; triethylamine; In diethyl ether; chloroform; acetonitrile;