Technology Process of 5-(3,5-Dimethoxy-2-nitro-benzyl)-6-methyl-7,8-dihydro-[1,3]dioxolo[4,5-g]isoquinolin-6-ium; iodide
There total 8 articles about 5-(3,5-Dimethoxy-2-nitro-benzyl)-6-methyl-7,8-dihydro-[1,3]dioxolo[4,5-g]isoquinolin-6-ium; iodide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
chloroform;
Heating;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: acide nitrique fumant, anhydride acetique / -20 °C
2: 98.5 percent / aq. KOH / methanol / 0.5 h / Heating
3: SOCl2, triethylamine / benzene / 3 h / Heating
4: triethylamine / diethyl ether
5: benzoate d'argent, triethylamine / diethyl ether; acetonitrile
6: Roblot F., Hocquemiller R., Cave A., J. Chem. Research (1989) (S) 344-345 (M) 2637-2651
7: 75 percent / CHCl3 / Heating
With
potassium hydroxide; thionyl chloride; acide nitrique fumant; benzoate d'argent; acetic anhydride; triethylamine;
In
methanol; diethyl ether; chloroform; acetonitrile; benzene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: SOCl2, triethylamine / benzene / 3 h / Heating
2: triethylamine / diethyl ether
3: benzoate d'argent, triethylamine / diethyl ether; acetonitrile
4: Roblot F., Hocquemiller R., Cave A., J. Chem. Research (1989) (S) 344-345 (M) 2637-2651
5: 75 percent / CHCl3 / Heating
With
thionyl chloride; benzoate d'argent; triethylamine;
In
diethyl ether; chloroform; acetonitrile; benzene;