1-(2,4-Dichloropyridin-3-YL)ethanone

Base Information

Chemical Name:1-(2,4-Dichloropyridin-3-YL)ethanone
CAS No.:1246349-89-2
Molecular Formula:C₇H₅Cl₂NO
Molecular Weight:190.029
Hs Code.:
European Community (EC) Number:846-140-3
DSSTox Substance ID:DTXSID10695002
Wikidata:Q82623974
Mol file:1246349-89-2.mol

Synonyms:1-(2,4-DICHLOROPYRIDIN-3-YL)ETHANONE;1246349-89-2;1-(2,4-dichloropyridin-3-yl)ethan-1-one;1-(2,4-Dichloro-pyridin-3-yl)-ethanone;Ethanone, 1-(2,4-dichloro-3-pyridinyl)-;SCHEMBL382884;DTXSID10695002;SDXMFHWBWDBSKR-UHFFFAOYSA-N;AMY17162;WZB34989;MFCD11847304;AKOS016009034;AS-39639;CS-0155131;EN300-109395;Z1255491582

Suppliers and Price of 1-(2,4-Dichloropyridin-3-YL)ethanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
1-(2,4-Dichloropyridin-3-yl)ethanone
100mg
$ 285.00

Chemenu
1-(2,4-dichloropyridin-3-yl)ethan-1-one 95%
1g
$ 297.00

American Custom Chemicals Corporation
1-(2,4-DICHLOROPYRIDIN-3-YL)ETHANONE 95.00%
5MG
$ 497.68

Ambeed
1-(2,4-Dichloropyridin-3-yl)ethanone 97%
1g
$ 193.00

Ambeed
1-(2,4-Dichloropyridin-3-yl)ethanone 97%
100mg
$ 112.00

Ambeed
1-(2,4-Dichloropyridin-3-yl)ethanone 97%
250mg
$ 112.00

Ambeed
1-(2,4-Dichloropyridin-3-yl)ethanone 97%
5g
$ 1112.00

Ambeed
1-(2,4-Dichloropyridin-3-yl)ethanone 97%
25g
$ 2400.00

Ambeed
1-(2,4-Dichloropyridin-3-yl)ethanone 97%
10g
$ 1658.00

Alichem
1-(2,4-Dichloropyridin-3-yl)ethanone
25g
$ 2840.80

Total 6 raw suppliers

Chemical Property of 1-(2,4-Dichloropyridin-3-YL)ethanone

Chemical Property:

Boiling Point:232.5±35.0 °C(Predicted)
PKA:-1.28±0.10(Predicted)
Density:1.376±0.06 g/cm3(Predicted)
Storage Temp.:under inert gas (nitrogen or Argon) at 2-8°C
XLogP3:2.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:188.9748192
Heavy Atom Count:11
Complexity:163

Purity/Quality:

HPLC≥98% ^*data from raw suppliers

1-(2,4-Dichloropyridin-3-yl)ethanone ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=O)C1=C(C=CN=C1Cl)Cl

Technology Process of 1-(2,4-Dichloropyridin-3-YL)ethanone

There total 3 articles about 1-(2,4-Dichloropyridin-3-YL)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1246349-88-1
1-(2,4-dichloropyridin-3-yl)ethan-1-ol

: 1246349-89-2
1-(2,4-dichloropyridin-3-yl)ethan-1-one

Guidance literature:: 1-(2,4-dichloropyridin-3-yl)ethan-1-ol; With 4-methylmorpholine N-oxide; In dichloromethane; for 0.25h; Molecular sieve;

With tetrapropylammonium perruthennate; In dichloromethane; at 20 ℃; for 2h;

Reference yield:

: 26452-80-2
2,4-dichloropyridine

: 1246349-89-2
1-(2,4-dichloropyridin-3-yl)ethan-1-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 2.5 h / -78 °C

1.2: 1.5 h / -78 °C

2.1: tetrahydrofuran / -78 - 20 °C

3.1: 4-methylmorpholine N-oxide / dichloromethane / 0.25 h / Molecular sieves 4?

3.2: 2 h / 20 °C

With n-butyllithium; 4-methylmorpholine N-oxide; diisopropylamine; In tetrahydrofuran; hexane; dichloromethane;

Reference yield:

: 134031-24-6
2,4-dichloro-3-pyridine Carboxaldehyde

: 1246349-89-2
1-(2,4-dichloropyridin-3-yl)ethan-1-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrahydrofuran / -78 - 20 °C

2.1: 4-methylmorpholine N-oxide / dichloromethane / 0.25 h / Molecular sieves 4?

2.2: 2 h / 20 °C

With 4-methylmorpholine N-oxide; In tetrahydrofuran; dichloromethane;