dicarbonyl(η4-tetraphenylcyclopentadienone)(trimethylamine)ruthenium

Base Information

Chemical Name:dicarbonyl(η4-tetraphenylcyclopentadienone)(trimethylamine)ruthenium
CAS No.:116335-24-1
Molecular Formula:C₃₄H₂₉NO₃Ru
Molecular Weight:600.679
Hs Code.:

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Chemical Property of dicarbonyl(η4-tetraphenylcyclopentadienone)(trimethylamine)ruthenium

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Technology Process of dicarbonyl(η4-tetraphenylcyclopentadienone)(trimethylamine)ruthenium

There total 2 articles about dicarbonyl(η4-tetraphenylcyclopentadienone)(trimethylamine)ruthenium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 12321-08-3
tricarbonyl(2,3,4,5-tetraphenylcyclopentadienone)ruthenium

: 1184-78-7
trimethylamine-N-oxide

: 116335-24-1
dicarbonyl(η4-tetraphenylcyclopentadienone)(trimethylamine)ruthenium

Guidance literature:: In benzene; a mixt. of Ru-complex and (CH3)3NO was refluxed under N2 in benzene for 24 h; the solvent was removed in vac.; elem. anal.;
DOI:10.1039/DT9870002815

Reference yield:

: 12321-08-3
tricarbonyl(2,3,4,5-tetraphenylcyclopentadienone)ruthenium

: 75-50-3
trimethylamine

: 116335-24-1
dicarbonyl(η4-tetraphenylcyclopentadienone)(trimethylamine)ruthenium

Guidance literature:: In water; toluene; mixture is stirred at room temp. for 3 h; solvent is removed in vacuo, the residue is extd. into CH2Cl2, fast chromy. on silica, elem. anal.;

Reference yield: 78.0%

: 116335-24-1
dicarbonyl(η4-tetraphenylcyclopentadienone)(trimethylamine)ruthenium

: 116363-15-6
(η(5)-2,3,4,5-tetraphenyl-1-methoxycyclopentadienyl)(iodo)dicarbonylruthenium(II)

Guidance literature:: With CH₃I; In benzene; Ru-complex and an excess of CH3I were refluxed under N2 in benzene for 24 h; the solvent was removed in vac., crystd. from Et2O; elem. anal.;
DOI:10.1039/DT9870002815