1-methyl-6-(N-benzoyl-DL-arginylamido)quinolinium diiodide

Base Information

Chemical Name:1-methyl-6-(N-benzoyl-DL-arginylamido)quinolinium diiodide
CAS No.:90606-03-4
Molecular Formula:C₂₃H₂₇N₆O₂*HI*I
Molecular Weight:674.323
Hs Code.:

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Chemical Property of 1-methyl-6-(N-benzoyl-DL-arginylamido)quinolinium diiodide

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Technology Process of 1-methyl-6-(N-benzoyl-DL-arginylamido)quinolinium diiodide

There total 4 articles about 1-methyl-6-(N-benzoyl-DL-arginylamido)quinolinium diiodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 84680-45-5
6-(N-benzoyl-DL-arginylamido)quinoline

: 74-88-4
methyl iodide

: 90606-03-4
1-methyl-6-(N-benzoyl-DL-arginylamido)quinolinium diiodide

Guidance literature:: In N,N-dimethyl-formamide; for 48h; Ambient temperature;
DOI:10.1021/jm00375a014

Reference yield:

: 580-15-4
6-aminoquinoline

: 90606-03-4
1-methyl-6-(N-benzoyl-DL-arginylamido)quinolinium diiodide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) isobutyl chloroformate, Et₃N / 1.) DMF, -20 deg C, 45 min, 2.) DMF, from -20 deg C to RT, 24 h

2: 77 percent / methanesulfonic acid, anisole / 0.67 h / Ambient temperature

3: 62 percent / dimethylformamide / 48 h / Ambient temperature

With methanesulfonic acid; methoxybenzene; triethylamine; isobutyl chloroformate; In N,N-dimethyl-formamide;
DOI:10.1021/jm00375a014

Reference yield:

: 90606-04-5
N-benzoyl-N-<(p-methoxyphenyl)sulfonyl>-L-arginine

: 90606-03-4
1-methyl-6-(N-benzoyl-DL-arginylamido)quinolinium diiodide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) isobutyl chloroformate, Et₃N / 1.) DMF, -20 deg C, 45 min, 2.) DMF, from -20 deg C to RT, 24 h

2: 77 percent / methanesulfonic acid, anisole / 0.67 h / Ambient temperature

3: 62 percent / dimethylformamide / 48 h / Ambient temperature

With methanesulfonic acid; methoxybenzene; triethylamine; isobutyl chloroformate; In N,N-dimethyl-formamide;
DOI:10.1021/jm00375a014