Felbamate Related Compound B (25 mg) (Phenethyl carbamate)

Base Information

• Chemical Name: Felbamate Related Compound B (25 mg) (Phenethyl carbamate)
• CAS No.: 6326-19-8
• Molecular Formula: C9H11 N O2
• Molecular Weight: 165.192
• Hs Code.: 2924296000
• Mol file: 6326-19-8.mol

Synonyms:Carbamicacid, phenethyl ester (8CI); NSC 31196; Phenethyl carbamate

Chemical Property of Felbamate Related Compound B (25 mg) (Phenethyl carbamate)

Chemical Property:

• PSA: 52.32000
• LogP: 2.02470

Purity/Quality:

98% ^*data from raw suppliers

PhenethylCarbamate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: Phenethyl Carbamate is an impurity in the synthesis of Felbamate (F231000), an antiepileptic, structurally similar to meprobamate.

Technology Process of Felbamate Related Compound B (25 mg) (Phenethyl carbamate)

There total 13 articles about Felbamate Related Compound B (25 mg) (Phenethyl carbamate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

2-phenylethanol (60-12-8) + urea (57-13-6) → 2-phenylethyl carbamate (6326-19-8)

Guidance literature:

With merrifield anchored iron(II)-anthra catalyst; In 1,4-dioxane; at 120 ℃; for 6.5h;

DOI:10.1039/c9nj05675k

Reference yield: 95.0%

2-phenylethanol (60-12-8) + potassium cyanate → 2-phenylethyl carbamate (6326-19-8)

Guidance literature:

With trifluoroacetic acid; In benzene; 1) 30 min.(addition); 2) 52 h, room temp.;

DOI:10.1135/cccc19800517

Reference yield: 90.0%

potassium cyanate (590-28-3) + 2-phenylethanol (60-12-8) → 2-phenylethyl carbamate (6326-19-8)

Guidance literature:

With para-dodecylbenzenesulfonic acid; In neat (no solvent); at 60 ℃; for 0.5h; Green chemistry;

DOI:10.1039/c5ra14528g

upstream raw materials:

2-phenylethanol

urea

sodium cyanide

sodium isocyanate

Downstream raw materials:

(5,11-Dihydro-10-thia-dibenzo[a,d]cyclohepten-5-yl)-carbamic acid phenethyl ester

4-phenyl-2-oxazolidinone

N-(cyclohex-2-enyl) phenethyl carbamate

C₉H₉Cl₂NO₂

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