3,3',5,5'-tetra(decyloxy)benzil

Base Information

Chemical Name:3,3',5,5'-tetra(decyloxy)benzil
CAS No.:1313574-90-1
Molecular Formula:C₅₄H₉₀O₆
Molecular Weight:835.305
Hs Code.:

Synonyms:

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Chemical Property of 3,3',5,5'-tetra(decyloxy)benzil

Chemical Property:

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Technology Process of 3,3',5,5'-tetra(decyloxy)benzil

There total 4 articles about 3,3',5,5'-tetra(decyloxy)benzil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17103-76-3
1,2-bis(3,5-dimethoxyphenyl)ethane-1,2-dione

: 1313574-90-1
3,3',5,5'-tetra(decyloxy)benzil

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen bromide; acetic acid / water / 5 h / Reflux

2: potassium carbonate / N,N-dimethyl-formamide / 18 h / Reflux

With hydrogen bromide; potassium carbonate; acetic acid; In water; N,N-dimethyl-formamide;
DOI:10.1002/ejic.201001288

Reference yield:

: 7311-34-4
3,5-dimethoxybenzaldehdye

: 1313574-90-1
3,3',5,5'-tetra(decyloxy)benzil

Guidance literature:: Multi-step reaction with 4 steps

1: sodium cyanide / ethanol; water / 36 h / Reflux

2: ammonium nitrate; copper diacetate; acetic acid / water / 2 h / Reflux

3: hydrogen bromide; acetic acid / water / 5 h / Reflux

4: potassium carbonate / N,N-dimethyl-formamide / 18 h / Reflux

With ammonium nitrate; sodium cyanide; hydrogen bromide; copper diacetate; potassium carbonate; acetic acid; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1002/ejic.201001288

Reference yield:

: 144758-76-9
1,2-bis-(3,5-dimethoxyphenyl)-2-hydroxyethanone

: 1313574-90-1
3,3',5,5'-tetra(decyloxy)benzil

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium nitrate; copper diacetate; acetic acid / water / 2 h / Reflux

2: hydrogen bromide; acetic acid / water / 5 h / Reflux

3: potassium carbonate / N,N-dimethyl-formamide / 18 h / Reflux

With ammonium nitrate; hydrogen bromide; copper diacetate; potassium carbonate; acetic acid; In water; N,N-dimethyl-formamide;
DOI:10.1002/ejic.201001288