3α-benzoyloxy-5α-cholestan-6-one

Base Information

Chemical Name:3α-benzoyloxy-5α-cholestan-6-one
CAS No.:86400-87-5
Molecular Formula:C₃₄H₅₀O₃
Molecular Weight:506.769
Hs Code.:

Synonyms:

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Chemical Property of 3α-benzoyloxy-5α-cholestan-6-one

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Technology Process of 3α-benzoyloxy-5α-cholestan-6-one

There total 9 articles about 3α-benzoyloxy-5α-cholestan-6-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 6579-82-4
3α-hydroxy-5α-cholestan-6-one

: 98-88-4
benzoyl chloride

: 86400-87-5
3α-benzoyloxy-5α-cholestan-6-one

Guidance literature:: In pyridine;
DOI:10.1248/cpb.35.986

Reference yield:

: 57-88-5
cholesterol

: 86400-87-5
3α-benzoyloxy-5α-cholestan-6-one

Guidance literature:: Multi-step reaction with 9 steps

2: 75 percent / 6 M hydrochloric acid / tetrahydrofuran / 1 h / Ambient temperature

3: 82 percent / pyridine / Ambient temperature

4: 75 percent / lithium aluminum hydride / tetrahydrofuran / 1 h / Ambient temperature

5: 91 percent / pyridine / Ambient temperature

6: 57 percent / butan-2-one / 20 h / Heating

7: 3.1 g / Jones reagent / acetone / 0.17 h / Ambient temperature

8: 72 percent / 5 percent potassium hydroxide / methanol / 3 h / Ambient temperature

9: 98 percent / pyridine

With hydrogenchloride; potassium hydroxide; lithium aluminium tetrahydride; jones reagent; In tetrahydrofuran; pyridine; methanol; acetone; butanone;
DOI:10.1248/cpb.35.986

Reference yield:

: 4470-73-9
5α-cholestane-3β,6β-diol 3-monoacetate

: 86400-87-5
3α-benzoyloxy-5α-cholestan-6-one

Guidance literature:: Multi-step reaction with 3 steps

1: 3.1 g / Jones reagent / acetone / 0.17 h / Ambient temperature

2: 72 percent / 5 percent potassium hydroxide / methanol / 3 h / Ambient temperature

3: 98 percent / pyridine

With potassium hydroxide; jones reagent; In pyridine; methanol; acetone;
DOI:10.1248/cpb.35.986