Technology Process of C35H50INO4Si
There total 12 articles about C35H50INO4Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: chloroform
2: hydrogen / palladium 10% on activated carbon / tetrahydrofuran
3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide; water
4: diisobutylaluminium hydride / dichloromethane
5: n-butyllithium / tetrahydrofuran
6: sodium carbonate / ethanol
7: Iodine monochloride / dichloromethane
With
n-butyllithium; hydrogen; Iodine monochloride; diisobutylaluminium hydride; sodium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
palladium 10% on activated carbon;
In
tetrahydrofuran; ethanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: hydrogen / palladium(II) hydroxide / ethyl acetate; tetrahydrofuran / 4.5 h / 760.05 Torr
2: 1H-imidazole / N,N-dimethyl-formamide / 1 h / 20 °C
3: dihydrogen peroxide; lithium hydroxide monohydrate / water; tetrahydrofuran / 2 h / 20 °C / Cooling with ice
4: triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide
5: n-butyllithium / tetrahydrofuran
6: sodium carbonate / ethanol
7: Iodine monochloride / dichloromethane
With
1H-imidazole; n-butyllithium; lithium hydroxide monohydrate; hydrogen; dihydrogen peroxide; Iodine monochloride; sodium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
palladium(II) hydroxide;
In
tetrahydrofuran; ethanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: hydrogen / palladium 10% on activated carbon / tetrahydrofuran
2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide; water
3: diisobutylaluminium hydride / dichloromethane
4: n-butyllithium / tetrahydrofuran
5: sodium carbonate / ethanol
6: Iodine monochloride / dichloromethane
With
n-butyllithium; hydrogen; Iodine monochloride; diisobutylaluminium hydride; sodium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
palladium 10% on activated carbon;
In
tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide;