C₂₀H₂₃NO

Base Information

Chemical Name:C₂₀H₂₃NO
CAS No.:1428660-48-3
Molecular Formula:C₂₀H₂₃NO
Molecular Weight:293.409
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₀H₂₃NO

Chemical Property:

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Technology Process of C₂₀H₂₃NO

There total 2 articles about C₂₀H₂₃NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3340-79-2
2-(o-methylphenyl)-1,2,3,4-tetrahydroisoquinoline

: 78-94-4,25038-87-3
methyl vinyl ketone

: 1428660-48-3
C₂₀H₂₃NO

Guidance literature:: With tris(bipyridine)ruthenium(II) dichloride hexahydrate; trifluoroacetic acid; In acetonitrile; at 50 ℃; for 72h; Schlenk technique; Inert atmosphere; Irradiation;
DOI:10.1021/jo400428m

Reference yield:

: 91-21-4
1,2,3,4-tetrahydroisoquinoline

: 95-46-5
2-methylphenyl bromide

: 1428660-48-3
C₂₀H₂₃NO

Guidance literature:: Multi-step reaction with 2 steps

1: 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium t-butanolate / toluene / 20 h / Inert atmosphere; Reflux

2: tris(bipyridine)ruthenium(II) dichloride hexahydrate; trifluoroacetic acid / acetonitrile / 72 h / 50 °C / Schlenk technique; Inert atmosphere; Irradiation

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tris(bipyridine)ruthenium(II) dichloride hexahydrate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; trifluoroacetic acid; sodium t-butanolate; In toluene; acetonitrile;
DOI:10.1021/jo400428m