[Cu2(.mu-I)2(η1-S-thiophene-2-carbaldehyde-N1-methyl semicarbazone)2(Ph3P)2]

Base Information

Chemical Name:[Cu2(.mu-I)2(η1-S-thiophene-2-carbaldehyde-N1-methyl semicarbazone)2(Ph3P)2]
CAS No.:1180863-95-9
Molecular Formula:C₅₀H₄₈Cu₂I₂N₆P₂S₄
Molecular Weight:1304.08
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Cu2(.mu-I)2(η1-S-thiophene-2-carbaldehyde-N1-methyl semicarbazone)2(Ph3P)2]

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Technology Process of [Cu2(.mu-I)2(η1-S-thiophene-2-carbaldehyde-N1-methyl semicarbazone)2(Ph3P)2]

There total 1 articles about [Cu2(.mu-I)2(η1-S-thiophene-2-carbaldehyde-N1-methyl semicarbazone)2(Ph3P)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 7681-65-4
copper(l) iodide

: 1434-96-4
thiophene-2-carbaldehyde N⁽¹⁾-methylthiosemicarbazone

: 603-35-0
triphenylphosphine

: 1180863-95-9
[Cu2(.mu-I)2(η1-S-thiophene-2-carbaldehyde-N1-methyl semicarbazone)2(Ph3P)2]

Guidance literature:: In acetonitrile; to soln. if copper(I) salt (1 equiv.) in MeCN thiosemicarbazone (1 equiv.) was added, stirred for 3-4 h, PPh3 was added, stirred for 5-10 min; slow evapd. at room temp., elem. anal.;
DOI:10.1016/j.ica.2009.03.043