4-phenoxycarbonyl-5-n-butylaminocarbonylimidazole

Base Information

• Chemical Name: 4-phenoxycarbonyl-5-n-butylaminocarbonylimidazole
• CAS No.: 474013-79-1
• Molecular Formula: C₁₅H₁₇N₃O₃
• Molecular Weight: 287.318

Synonyms:

Chemical Property of 4-phenoxycarbonyl-5-n-butylaminocarbonylimidazole

Chemical Property:

Purity/Quality:

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Technology Process of 4-phenoxycarbonyl-5-n-butylaminocarbonylimidazole

There total 3 articles about 4-phenoxycarbonyl-5-n-butylaminocarbonylimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4H,9H-diimidazo<1,5-a; 1',5'-d>pyrazine-5,10-dione-1,6-dicarboxylic dichloride (59157-06-1) → 4-phenoxycarbonyl-5-n-butylaminocarbonylimidazole (474013-79-1)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / CH₂Cl₂ / 1 h / 0 °C

2: 4.11 g / tetrahydrofuran / 1.5 h / -40 °C

With pyridine; In tetrahydrofuran; dichloromethane;

DOI:10.1021/jo025536c

Reference yield:

4,5-imidazoledicarboxylic acid (570-22-9) → 4-phenoxycarbonyl-5-n-butylaminocarbonylimidazole (474013-79-1)

Guidance literature:

Multi-step reaction with 3 steps

1: thionyl chloride; DMF / benzene / 16 h / Heating

2: pyridine / CH₂Cl₂ / 1 h / 0 °C

3: 4.11 g / tetrahydrofuran / 1.5 h / -40 °C

With pyridine; thionyl chloride; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; benzene;

DOI:10.1021/jo025536c

Reference yield:

N-butylamine (109-73-9,85404-21-3) + 5,10-dioxo-5H,10H-diimidazolo[1,5-a:1',5'-d]pyrazine-1,6-dicarboxylic acid diphenyl ester (474013-77-9) → 4-phenoxycarbonyl-5-n-butylaminocarbonylimidazole (474013-79-1)

Guidance literature:

In tetrahydrofuran; at -40 ℃; for 1.5h;

DOI:10.1021/jo025536c

upstream raw materials:

N-butylamine

5,10-dioxo-5H,10H-diimidazolo[1,5-a:1',5'-d]pyrazine-1,6-dicarboxylic acid diphenyl ester

4H,9H-diimidazo<1,5-a; 1',5'-d>pyrazine-5,10-dione-1,6-dicarboxylic dichloride

4,5-imidazoledicarboxylic acid

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