[(C₅Me₅)2Ru₂Cl(PhP(C₆H₄-o-S)2)]Cl*dichloromethane

Base Information

• Chemical Name: [(C₅Me₅)2Ru₂Cl(PhP(C₆H₄-o-S)2)]Cl*dichloromethane
• CAS No.: 1255070-52-0
• Molecular Formula: CH₂Cl₂*C₃₈H₄₃ClPRu₂S₂*Cl
• Molecular Weight: 952.844
• Mol file: 1255070-52-0.mol

Synonyms:

Chemical Property of [(C₅Me₅)2Ru₂Cl(PhP(C₆H₄-o-S)2)]Cl*dichloromethane

Chemical Property:

Purity/Quality:

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Technology Process of [(C₅Me₅)2Ru₂Cl(PhP(C₆H₄-o-S)2)]Cl*dichloromethane

There total 1 articles about [(C₅Me₅)2Ru₂Cl(PhP(C₆H₄-o-S)2)]Cl*dichloromethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

bis[dichloro(pentamethylcyclopentadienyl)ruthenium(III)] + dichloromethane (75-09-2) + [(pentamethylcyclopentadienyl)Ru{PhP(C6H4-o-S)2}] (1254784-42-3) → [(C5Me5)2Ru2Cl(PhP(C6H4-o-S)2)]Cl*dichloromethane (1255070-52-0)

Guidance literature:

In dichloromethane; (inert atm., Schlenk technique); stirring mixt. of ruthenium compds. at room temp. for 20 h; evapn., washing with THF, recrystn. (CH2Cl2/hexane), NMR;

DOI:10.1021/om100852x

upstream raw materials:

dichloromethane

[(pentamethylcyclopentadienyl)Ru{PhP(C₆H₄-o-S)₂}]

Refernces