Technology Process of C25H26Br3N3O4
There total 8 articles about C25H26Br3N3O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C26H30Br4N2O6;
With
hydrogenchloride;
In
1,4-dioxane;
at 20 ℃;
for 4h;
morpholine;
In
tetrahydrofuran;
at 20 ℃;
DOI:10.1016/j.bmcl.2013.07.017
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 36 h / 20 °C
2.1: bromine / chloroform / 2 h / 20 °C
3.1: chloroform / 18 h / 20 °C
4.1: hydrogen bromide; water / methanol / 48 h
5.1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 4 h
6.1: hydrogenchloride / 1,4-dioxane / 4 h / 20 °C
6.2: 20 °C
With
hydrogenchloride; water; hydrogen bromide; bromine; potassium carbonate; triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate;
In
1,4-dioxane; methanol; chloroform; N,N-dimethyl-formamide;
3.1: |Delepine Amine Synthesis;
DOI:10.1016/j.bmcl.2013.07.017
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 4 h
2.1: hydrogenchloride / 1,4-dioxane / 4 h / 20 °C
2.2: 20 °C
With
hydrogenchloride; triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate;
In
1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.07.017
