(THF)3Li(OCN(iPr)2(C₆H₄)triisobutylaluminate

Base Information

Chemical Name:(THF)3Li(OCN(iPr)2(C₆H₄)triisobutylaluminate
CAS No.:1004325-02-3
Molecular Formula:C₃₇H₆₉AlLiNO₄
Molecular Weight:625.882
Hs Code.:

(THF)3Li(OCN(iPr)2(C<sub>6</sub>H<sub>4</sub>)triisobutylaluminate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (THF)3Li(OCN(iPr)2(C₆H₄)triisobutylaluminate

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Technology Process of (THF)3Li(OCN(iPr)2(C₆H₄)triisobutylaluminate

There total 1 articles about (THF)3Li(OCN(iPr)2(C₆H₄)triisobutylaluminate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 109-72-8,29786-93-4
n-butyllithium

: 20383-28-2
N,N-diisopropyl benzamide

: 100-99-2,130565-62-7
triisobutylaluminum

: 1004325-02-3
(THF)3Li(OCN(iPr)2(C₆H₄)triisobutylaluminate

: 1004325-01-2
Li(THF)4 tetraisobutylaluminate

Guidance literature:: With 2,2,6,6-tetramethylpiperidine; In tetrahydrofuran; hexane; (Ar), stoich., BuLi in hexane added to mixt. of THF and TMPH at -78°C, stirred at 0°C for 10 min, treated with Al complex in hexane at -78°C, stirred for 30 min at 0°C, treated with benzamide at -78°C, stirred at room; cooled, evapd.(vac.), treated with hexane, cooled to -27°C, elem.anal.;
DOI:10.1039/b713913f