o-ethylbenzyltrimethylgermane

Base Information

Chemical Name:o-ethylbenzyltrimethylgermane
CAS No.:76283-22-2
Molecular Formula:C₁₂H₂₀Ge
Molecular Weight:236.881
Hs Code.:

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Suppliers and Price of o-ethylbenzyltrimethylgermane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of o-ethylbenzyltrimethylgermane

Chemical Property:

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Technology Process of o-ethylbenzyltrimethylgermane

There total 2 articles about o-ethylbenzyltrimethylgermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 917-64-6
methyl magnesium iodide

: germanium(II) chloride dioxane

: 53201-06-2
p-EtC₆H₅CH₂

: 53201-07-3
6-methylene-1-ethyl-2,4-cyclohexadiene

: 76283-22-2
o-ethylbenzyltrimethylgermane

: 76283-23-3
p-ethylbenzyltrimethylgermane

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; diethyl ether; an ether soln. of triens was added to refluxing GeCl2*C4H8O2 in THF, mixt. then treated with HCl and MeMgI was added; aq. NH4Cl was added, product was extd. with ether;;

Reference yield:

: 917-64-6
methyl magnesium iodide

: 76283-21-1
p-ethylbenzyltrichlorogermane

: 76283-27-7
o-ethylbenzyltrichlorogermane

: 76283-22-2
o-ethylbenzyltrimethylgermane

: 76283-23-3
p-ethylbenzyltrimethylgermane

Guidance literature:: With ammonium chloride; In diethyl ether; to a soln. of isomers in ether was added with stirring over 2 h MeMgI in ether, after boiling for 8 h the mixt. was treated with aq. NH4Cl; ether layer was removed and dried over CaCl2, product was isolated by distillation at 110-113°C; NMR;