p-ethylbenzyltrichlorogermane

Base Information

Chemical Name:p-ethylbenzyltrichlorogermane
CAS No.:76283-21-1
Molecular Formula:C₉H₁₁Cl₃Ge
Molecular Weight:298.135
Hs Code.:

Synonyms:

Suppliers and Price of p-ethylbenzyltrichlorogermane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-ethylbenzyltrichlorogermane

Chemical Property:

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Technology Process of p-ethylbenzyltrichlorogermane

There total 1 articles about p-ethylbenzyltrichlorogermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: germanium(II) chloride dioxane

: 1467-05-6
4-ethylbenzylchloride

: 1467-06-7
2-ethylbenzyl chloride

: 76283-21-1
p-ethylbenzyltrichlorogermane

: 76283-27-7
o-ethylbenzyltrichlorogermane

Guidance literature:: In not given; GeCl2*C4H8O2 was added to mixt. og reagents, the soln. was heated for 8h at 130°C; product was isolated by distillation at 120-123°C (mixt. of o- and p-isomers); NMR;

Reference yield:

: 917-64-6
methyl magnesium iodide

: 76283-21-1
p-ethylbenzyltrichlorogermane

: 76283-27-7
o-ethylbenzyltrichlorogermane

: 76283-22-2
o-ethylbenzyltrimethylgermane

: 76283-23-3
p-ethylbenzyltrimethylgermane

Guidance literature:: With ammonium chloride; In diethyl ether; to a soln. of isomers in ether was added with stirring over 2 h MeMgI in ether, after boiling for 8 h the mixt. was treated with aq. NH4Cl; ether layer was removed and dried over CaCl2, product was isolated by distillation at 110-113°C; NMR;