4H-[1,2,4]Triazolo[4,3-a][1,4]benzodiazepine,1-methyl-6-phenyl-

Base Information

Chemical Name:4H-[1,2,4]Triazolo[4,3-a][1,4]benzodiazepine,1-methyl-6-phenyl-
CAS No.:28910-92-1
Molecular Formula:C17H14 N4
Molecular Weight:274.325
Hs Code.:

Synonyms:4H-s-Triazolo[4,3-a][1,4]benzodiazepine,1-methyl-6-phenyl- (8CI); 1-Methyl-6-phenyl-4H-s-triazolo[4,3-a][1,4]benzodiazepine;U 31957

Suppliers and Price of 4H-[1,2,4]Triazolo[4,3-a][1,4]benzodiazepine,1-methyl-6-phenyl-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4H-[1,2,4]Triazolo[4,3-a][1,4]benzodiazepine,1-methyl-6-phenyl-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4H-[1,2,4]Triazolo[4,3-a][1,4]benzodiazepine,1-methyl-6-phenyl-

There total 2 articles about 4H-[1,2,4]Triazolo[4,3-a][1,4]benzodiazepine,1-methyl-6-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 28981-97-7
alprazolam

U 31957: 28910-92-1
U 31957

: 36916-19-5
5-chloro-2-(3-methyl-4H-1,2,4-triazol-4-yl)benzophenone

: 448950-89-8
triazolaminoquinoleine

Guidance literature:: With hydrogenchloride; In water; for 8h; pH=3.6; Further Variations:; pH-values; Kinetics; UV-irradiation;
DOI:10.1002/poc.861

Reference yield:

U 31957: 28910-92-1
U 31957

Guidance literature:: Acethydrazid,1,3-Dihydro-5-phenyl-2H-1,4-benzodiazepin-2-thion(19);
DOI:10.1021/jm00293a015

Reference yield: 48.0%

U 31957: 28910-92-1
U 31957

: 105-36-2
ethyl bromoacetate

: 1300746-54-6
ethyl (1-methyl-6-phenyl-4H-[1,2,4]triazolo[4,3-a][1,4]benzodiazepin-4-yl)acetate

Guidance literature:: U 31957; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.25h;

ethyl bromoacetate; In tetrahydrofuran; at -78 - 20 ℃; for 24h;
DOI:10.1021/jm401088k