C₂₃H₁₅N₃O

Base Information

Chemical Name:C₂₃H₁₅N₃O
CAS No.:380918-53-6
Molecular Formula:C₂₃H₁₅N₃O
Molecular Weight:349.392
Hs Code.:

C<sub>23</sub>H<sub>15</sub>N<sub>3</sub>O

Synonyms:

Suppliers and Price of C₂₃H₁₅N₃O

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of C₂₃H₁₅N₃O

Chemical Property:

Purity/Quality:: 95%+ or 98%+ ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₃H₁₅N₃O

There total 4 articles about C₂₃H₁₅N₃O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 1415212-82-6
5-bromo-3-(3-cyanophenyl)-1-phenyl-1,2-dihydropyridin-2-one

: 17997-47-6
2-tri-n-butylstannylpyridine

: 380918-53-6
C₂₃H₁₅N₃O

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide;
DOI:10.1021/jm301268u

Reference yield:

: 1072-97-5
5-bromo-2-pyridylamine

: 380918-53-6
C₂₃H₁₅N₃O

Guidance literature:: Multi-step reaction with 5 steps

1.1: sulfuric acid; iodine / water; acetic acid / 6 h / 80 °C

2.1: sulfuric acid / 2 h / 20 °C / Cooling with ice

2.2: 72 h / 20 °C

3.1: triethylamine; copper diacetate / dichloromethane / 120 h / 20 °C

4.1: caesium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 2 h / 80 °C / Inert atmosphere

5.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sulfuric acid; iodine; copper diacetate; caesium carbonate; triethylamine; In dichloromethane; water; acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/jm301268u

Reference yield:

: 381233-96-1
2-amino-3-iodo-5-bromopyridine

: 380918-53-6
C₂₃H₁₅N₃O

Guidance literature:: Multi-step reaction with 4 steps

1.1: sulfuric acid / 2 h / 20 °C / Cooling with ice

1.2: 72 h / 20 °C

2.1: triethylamine; copper diacetate / dichloromethane / 120 h / 20 °C

3.1: caesium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 2 h / 80 °C / Inert atmosphere

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sulfuric acid; copper diacetate; caesium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm301268u